Whitten, Davis, and Peck, General Chemistry, 6th Edition
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| |Recommended CER Experiments |
| |to accompany |
| |Hornback’s Organic Chemistry, Second Edition |
| | |
| |The table below matches sections from the book with recommended CER labs. Click on the experiment title to view a PDF of each lab. Go to to search the complete CER database and to learn more |
| |about customizing your lab manual through CER. To access password-protected material, like instructor’s resources and printable review copies on this site, contact Rebecca Heider for a password. |
| | |
|Chapter Title |Recommended Experiment(s) from CER |
|2. Organic Compounds: A First Look |ANAL 735: Catalytic Hydrogenation of Unknowns |
|6. Stereochemistry I |SYNT 719: Brominating Alkenes |
|Cis-Trans Isomers and Conformations |REAC 734: Molecular Rearrangement Reactions: Azobenzene and Benzilic Acid |
|7. Stereochemistry |SYNT 719: Brominating Alkenes |
|II |REAC 734: Molecular Rearrangement Reactions: Azobenzene and Benzilic Acid |
|Chiral Molecules |ANAL 751: Enantiomeric Purity of Commercial Ibuprofen |
| |TECH 752: Resolving a Racemic Mixture: Using (-)-Proline to Separate (±)-Phenylsuccinic Acid |
|8. Nucleophilic Substitution Reactions |REAC 714: Studying SN1 and SN2 Reactions: Nucleophilic Substitution |
|Reactions of Alkyl Halides, Alcohols, and |KINE 733: The Kinetics of Solvolysis of 2-Chloro-2-Methylpropane |
|Related Compounds | |
|9. Elimination Reactions |REAC 712: Dehydrating Cyclohexanol |
|Reactions of Alkyl Halides, Alcohols, and |REAC 736: The Pinacol Rearrangement |
|Related Compounds | |
| |SYNT 713: Preparing Isopentylacetate by the Fischer Esterification |
| |SYNT 725: Oxidizing Methoxybenzyl Alcohol to Methoxybenzaldehyde Using Phase Transfer Catalysis |
|10. Synthetic Uses of Substitution and |SYNT 726: Two Methods for the Synthesis of Phenacetin |
|Elimination Reactions |SYNT 738: Copper-Catalyzed Oxidation of Benzoin to Benzil |
|Interconverting Functional Groups |REAC 742: Acid-Catalyzed Hydration of 1-Hexene to Make 2-Hexanol |
| |SYNT 745: Synthesizing Aspirin: The Acetylation of Salicylic Acid |
| |SYNT 746: Acetaminophen: The Acetylation of p-Aminophenol |
| |REAC 747: Hydroboration and Oxidation of 1Hexene to Make 1Hexanol |
|11. Additions of Carbon-Carbon Double and |SYNT 719: Brominating Alkenes |
|Triple Bonds |REAC 742: Acid-Catalyzed Hydration of 1-Hexene to Make 2-Hexanol |
|Reactions of Alkenes and Alkynes |REAC 747: Hydroboration and Oxidation of 1Hexene to Make 1Hexanol |
|17. Aromatic Substitution Reactions |REAC 716: Nitrating Acetanilide or Methyl Benzoate: Electrophilic Aromatic Substitution |
| |SYNT 723: Friedel-Crafts Acylation: Synthesis of 4-Methoxyacetophenone |
| |SYNT 724: Friedel-Crafts Alkylation: Kinetic versus Thermodynamic Control |
| |SYNT 748: Formation of Benzyne and Its Diels-Alder Reaction: A Multistep Reaction Sequence |
| |REAC 749: Nucleophilic Aromatic Substitution: The Reaction of 3,4-Dichloronitrobenzene with Sodium Methoxide |
|18. Additions to the Carbonyl Group |REAC 715: Reducing Benzil Using Sodium Borohydride |
|Reactions of Aldehydes and Ketones |SYNT 718: Nucleophilic Addition to Carbonyl: Grignard Reaction with an Aldehyde |
| |REAC 721: Synthesis of Trans-9-(2-Phenylethenyl)Anthracene: A Wittig Reaction |
| |SYNT 743: Converting Benzaldehyde to Benzilic Acid: A Multistep Synthesis |
| |REAC 750: Cannizzaro Reaction: The Conversion of p-Nitrobenzaldehyde into p-Nitrobenzoic Acid and p-Nitrobenzyl Alcohol |
|19. Substitutions at the Carbonyl Group |SYNT 713: Preparing Isopentylacetate by the Fischer Esterification |
|Reactions of Carboxylic Acids and |SYNT 726: Two Methods for the Synthesis of Phenacetin |
|Derivatives |SYNT 737: Thiamine-Catalyzed Benzoin Condensation |
| |SYNT 743: Converting Benzaldehyde to Benzilic Acid: A Multistep Synthesis |
| |SYNT 745: Synthesizing Aspirin: The Acetylation of Salicylic Acid |
| |SYNT 746: Acetaminophen: The Acetylation of p-Aminophenol |
|20. Enolate and Other Carbon Nucleophiles |SYNT 720: The Aldol Condensation: Synthesis of Dibenzalacetone |
| |SYNT 737: Thiamine-Catalyzed Benzoin Condensation |
| |SYNT 754: A Multistep Synthesis Sequence: An Aldol Condensation, a Michael Addition, and Ethylene Ketal Formation |
|21. The Chemistry of Radicals |REAC 741: Free Radical Chlorination |
|22. Carbonyl Alpha-Substitution Reactions |SYNT 717: The Diels-Alder Reaction of Anthracene with Maleic Anhydride |
| |SYNT 748: Formation of Benzyne and Its Diels-Alder Reaction: A Multistep Reaction Sequence |
|23. Carbonyl Condensation Reactions |SYNT 720: The Aldol Condensation: Synthesis of Dibenzalacetone |
| |SYNT 737: Thiamine-Catalyzed Benzoin Condensation |
| |SYNT 754: A Multistep Synthesis Sequence: An Aldol Condensation, a Michael Addition, and Ethylene Ketal Formation |
|24. Synthetic Polymers |SYNT 739: The Synthesis of a Superabsorbent Polymer |
|25. Carbohydrates |SYNT 713: Preparing Isopentylacetate by the Fischer Esterification |
|Recommended Techniques from CER |
|TECH 700: Practicing Safety in the Organic Chemistry Laboratory |
|TECH 701: Measuring the Melting Points of Compounds and Mixtures |
|TECH 702: Using Microscale Techniques |
|TECH 703: Purifying Acetanilide by Recrystallization |
|TECH 704: Separating Cyclohexane and Toluene by Distillation |
|TECH 705: Separating Acids and Neutral Compounds of Solvent Extraction |
|TECH 706: Separating Camphor from BetaCarotene by Sublimation |
|TECH 707: Separating a Mixture by Thin-Layer Chromatography |
|TECH 708: Separating Ferrocene and Acetylferrocene by Adsorption Column Chromatography |
|TECH 709: Separating and Identifying Mixtures by Gas Chromatography |
|TECH 710: Identifying an Unknown Compound by Infrared Spectroscopy |
|TECH 711: Using NMR Spectroscopy to Identify an Unknown Organic Compound |
|TECH 722: Isolating Clove Oil from Cloves Using Steam Distillation |
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