Analysis for Residential Pesticides in Surface Water
For analysis of Clopyralid, Dicamba, 2, 4-D, Triclopyr, and MCPP, acidify 500 ml of an approximately room temperature sample to pH 2 using phosphoric acid. Run this sample through the cartridge at approximately 25 kPa. Dry cartridge completely (approximately one hour) and elute with 5 ml methanol:methyl-t-butyl ether (10:90). Dry this completely and reconstitute in 0.5 ml HPLC water. Sonicate ... ................
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