WA7890008967 Part III, Operating Unit Group 4 242-A Evaporator 1 ADDENDUM B

WA7890008967 Part III, Operating Unit Group 4 242-A Evaporator

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ADDENDUM B

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WASTE ANALYSIS PLAN

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Part III, Operating Unit Group 4-B.i

WA7890008967 Part III, Operating Unit Group 4 242-A Evaporator

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Part III, Operating Unit Group 4-B.ii

WA7890008967 Part III, Operating Unit Group 4 242-A Evaporator

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ADDENDUM B

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WASTE ANALYSIS PLAN

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4 Contents

5 B

WASTE ANALYSIS PLAN ......................................................................................................B.1

6 B.1 Introduction ................................................................................................................................B.1

7 B.2 Purpose .......................................................................................................................................B.1

8 B.3 Scope ..........................................................................................................................................B.1

9 B.4 242-A Evaporator Process Description ......................................................................................B.1

10 B.5 Waste Feed Identification...........................................................................................................B.3

11 B.5.1 General Constituent Description ................................................................................................B.3

12 B.5.2 Classification of Waste...............................................................................................................B.3

13 B.5.3 Dangerous Waste Numbers ........................................................................................................B.4

14 B.6 Waste Acceptance Process .........................................................................................................B.4

15 B.7 Waste Feed Acceptance Process ................................................................................................B.5

16 B.7.1 Identification of Candidate Waste Feed .....................................................................................B.6

17 B.7.2 Candidate Waste Feed Acceptance ............................................................................................B.6

18 B.8 Secondary Waste Sampling and Analysis ..................................................................................B.7

19 B.8.1 Process Condensate Waste Sampling Process............................................................................B.7

20 B.9 Process Control Aqueous Waste Sampling and Analysis ..........................................................B.8

21 B.10 242-A Evaporator Acceptance Criteria ......................................................................................B.8

22 B.10.1 Candidate Feed Tank Waste Acceptance Criteria ......................................................................B.8

23 B.11 Sample Collection and Analysis.................................................................................................B.9

24 B.11.1 Candidate Feed Tank Sampling and Analysis............................................................................B.9

25 B.11.2 Process Condensate Sampling and Analysis ............................................................................B.11

26 B.11.3 Analyte Selection and Rationale ..............................................................................................B.12

27 B.12 Analytical Methods and Quality Assurance and Quality Control ............................................B.14

28 B.12.1 Laboratory Selection ................................................................................................................B.14

29 B.12.2 Analytical Methods ..................................................................................................................B.14

30 B.13 References ................................................................................................................................B.15

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Part III, Operating Unit Group 4-B.iii

1 Figures and Tables

WA7890008967 Part III, Operating Unit Group 4 242-A Evaporator

2 3 Figure B.1. 242-A Evaporator Simplified Schematic ...............................................................................B.2 4 Table B.1. Waste Designation for Process Condensate ............................................................................B.4 5 Figure B.2. 242-A Evaporator Waste Acceptance Process.......................................................................B.5 6 Table B.2. Candidate Feed Tank Sample Point Selection ......................................................................B.13 7 Table B.3. Analytes for Candidate Feed Tanks ......................................................................................B.13 8 Table B.4. Analytical Methods for Candidate Feed Tank Stream Analytes ...........................................B.15 9 10

Part III, Operating Unit Group 4-B.iv

1 ACRONYMS

2 ASTM 3 AWWA 4 CFR 5 CT 6 DOE 7 DSC 8 DST 9 Ecology 10 ETF 11 GC 12 HDPE 13 IC 14 ICT 15 IR 16 LDR 17 LERF 18 MS 19 N/A 20 QA 21 QC 22 RPD 23 TEDF 24 TCLP 25 TOC 26 TSD 27 VOA 28 WAC 29 WAP

WA7890008967 Part III, Operating Unit Group 4 242-A Evaporator

American Society for Testing and Materials American Water Works Association Code of Federal Regulations total carbon U. S. Department of Energy differential scanning calorimeter Double-Shell Tanks Washington State Department of Ecology 200 Area Effluent Treatment Facility gas chromatography high-density polyethylene Ion Chromatography total inorganic carbon infrared land disposal restriction Liquid Effluent Retention Facility mass spectrometry not applicable quality assurance quality control relative percent difference Treated Effluent Disposal Facility toxicity characteristic leaching procedure total organic carbon treatment, storage, and/or disposal volatile organic analysis Washington Administrative Code waste analysis plan

Part III, Operating Unit Group 4-B.v

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