Year 4 draft FSIS Final Nov 2015 - Food Standards Agency



Food Survey Information Sheet November 2015Surveillance programme for Mycotoxins in foodsYear 4: Surveillance programme for rarely tested for mycotoxinsSummary ? 400 samples of foods were collected and analysed from a range of food categories including: spices, fruit, fruit juices, cereal, vegetable, alcohol, oil, seeds, nuts and dairy. ? A total of 23 mycotoxins including citrinin, alternaria toxins, fumonisins, sterigmatocystin and the ergot alkaloids were included in the fourth year of the surveillance programme. ? The levels of mycotoxins found in this survey were low and indicate no appreciable risk to the health of the general population from exposure to mycotoxins from these products. ? The FSA's advice is that there is no need for consumers to change their eating habits with respect to the foods sampled. ? The data generated from this survey will be submitted to EFSA in the future to contribute to their risk assessments. Background 1. The Food Standards Agency (FSA) has a 4 year rolling programme of surveys which investigate the presence of mycotoxins in a range of foods. The fourth year of the programme looked at the presence of mycotoxins that are less commonly tested for in a range of food products with the potential to be contaminated with such mycotoxins. 2. Mycotoxins are a group of naturally occurring chemicals produced by certain moulds. They can grow on a variety of different crops and foodstuffs including cereals, nuts and spices during production and subsequent storage1, 2.3. Mycotoxins studied in this survey include citrinin, alternaria toxins, fumonisins, sterigmatocystin and ergot alkaloids. The safety evaluation of mycotoxins 4. Mycotoxins have been shown to cause a range of adverse health effects in animals and there is a concern that these effects may also occur in humans if high levels of mycotoxins are consumed over long periods of time. 5. The European Food Safety Authority (EFSA), which assesses and communicates on all risks associated with the food chain, its predecessor the European Scientific Committee on Food (SCF)3, 4 and the Joint FAO/WHO Expert Committee on Food Additives (JECFA) have published opinions on the toxicity of some mycotoxins including ergot alkaloids5, fumonisins6, citrinin7, sterigmatocystin8 and alternaria toxins9. 6. For many mycotoxins, a tolerable daily intake (TDI) or a tolerable weekly intake (TWI) has been established, which is a toxicological guideline value for the quantity of a particular type of mycotoxin that someone can be exposed to daily or weekly over a lifetime without it posing a significant risk to health. The law on mycotoxins 7. Some mycotoxins, such as aflatoxins and patulin, are covered by European Union (EU) legislation. This legislation sets maximum levels for the amount of a specific mycotoxin permitted in a specific food type. 8. In order to protect consumer health, regulatory controls for aflatoxins, ochratoxin A, ergot alkaloids and Fusarium toxins in certain foodstuffs are set out in European Union (EU) legislation, specifically Commission Regulation (EC) No. 1881/2006, as amended10. It is the responsibility of food businesses to ensure that products they place on the market are compliant with food safety legislation, including maximum levels for mycotoxins.9. Those mycotoxins not covered by EU legislation which are included in the fourth year of the survey have been analysed and where positive levels were found, the risk from these has been assessed. FSA mycotoxin surveys: aims and previous work 10. The FSA carries out surveillance for the following reasons: - to determine the levels of mycotoxins in certain food groups for use in risk assessments; - to generate data on occurrence of key mycotoxins in foods to enable informed negotiations in Brussels and other international fora; - to determine the occurrence of mycotoxins for which there are no regulatory limits and/or for which there are limited data; and - to identify emerging areas of possible concern. 11. The first year of the four-year surveillance programme investigated the presence of a range of mycotoxins in a number of cereal-based retail foods. The food products ranged from staple cereal products through to speciality products which contain principal cereal ingredients known to be susceptible to mycotoxin contamination. The results of this work were published in 201011. 12. The second year of the surveillance programme comprised the following three surveys, and the results of this work were published in 201212: - Mycotoxins in food products for infants and young children (Survey 1) - Ergot alkaloids in cereals and cereal products (Survey 2) - Patulin in apple juice (Survey 3) 13. The third year of the surveillance programme aimed to investigate the occurrence of mycotoxins in a range of ethnic foods available on the UK market and the results of this work were published in 201313.Fourth year of the survey14. The fourth year of the surveillance programme investigated a range of mycotoxins in a variety of food products with the potential to be contaminated with mycotoxins. The mycotoxins tested for included: citrinin, alternaria toxins, fumonisins, sterigmatocystin and ergot alkaloids. The food products analysed include spices, fruit, fruit juices, cereals, vegetables, alcohol, oil, seeds, nuts, and dairy products which contain principal ingredients known to be susceptible to mycotoxin contamination. Methodology and Reporting Sampling 15. A total of 400 samples were collected on behalf of the Food Standards Agency by Ventress Technical Limited. Samples were purchased from a full range of retail outlets including major and smaller national supermarkets, independent and specialist retailers, farmers markets, ethnic supermarkets, online retailers and licensed market stalls. Detailed documentations ensured traceability of all products purchased. The samples were delivered to Premier Analytical Services (PAS) at ambient temperature and stored at –16°C until required for analysis. Full details of the samples are shown in Appendix 1, table 1. 16. All samples in this survey were ground and thoroughly mixed to ensure homogeneity prior to analysis. After homogenisation each sample was split equally between three containers, ‘A’, ‘B’ and ‘C’ and stored in a freezer at –16°C. Sub-sample ‘A’ was used for the analysis and sub-samples ‘B’ and ‘C’ were kept frozen; one for analysis by the retailer at their request and the other for referee purposes. Samples were allowed to defrost to ambient temperature prior to analysis and any remaining sample returned to –16°C immediately after analysis. Analysis 17. The analysis for mycotoxins in cereals and cereal products was conducted using fully validated United Kingdom Accreditation Service (UKAS) accredited methods. 18. All analyses were performed by PAS trained staff in a UKAS accredited laboratory operating an internal audit and review process. On-going control of mycotoxin analyses at PAS laboratories is monitored using in-house naturally contaminated test materials and by participation in Food Analysis Performance Assessment Scheme (FAPAS) and intercomparison/collaborative studies, when available.19. All test results were obtained from methods that use internal standards for recovery correction and reported with the corresponding measurement uncertainty (MU), in line with the Agency Guidelines and European Union legislation. 20. For this survey the calculation of the MU was carried out using in-house data, performance in international collaborative trials and the FAPAS thus incorporating repeatability and reproducibility data. 21. The expanded MU was calculated using a standard coverage factor of 2, equivalent to a confidence of approximately 95 percent. MU figures for each of the mycotoxins can be found in Appendix 4 Table 1. 22. All analyses were conducted with spiked samples i.e. a known amount of toxin was added to each sample matrix on each day prior to extraction. These samples were used to assess recovery and recoveries between 70% and 110% were classed as valid. Spiked samples were also used for quantification and all results were corrected for recovery. Recovery data from throughout the study are shown in Appendix 4, Table 2. 23. Additional information on methods and determination limits can be found in Table 3 in Appendix 4 and in more detail in the contractor’s final report. Results, discussion and action taken 24. Details of the samples purchased, including brand names, batch numbers and best before dates (where available) and the retail outlets from which the samples were obtained are provided in Appendix 1. 25. Levels of mycotoxins were low in the majority of the 400 samples analysed. The results of the survey are summarised in Appendix 2. 26. For each individual sample, the number of mycotoxins analysed ranged from 1 to 23, depending on the food type. 27. The individual results are listed in Appendix 2. Tables 1 and 2 in Appendix 3 summarises the occurrence of the individual mycotoxins.Citrinin28. Citrinin is a mycotoxin found in stored grains in addition to plant products such as beans, fruits, fruit and vegetable juices, herbs, spices and spoiled dairy products. Co-occurrence of citrinin with aflatoxin and ochratoxin A is common, since the fungi procuding these toxins are the same. Citrinin has been shown to affect the liver and kidneys in animals. The potential for carcinogenicity has not been adequately investigated. 29. Citrinin was detected in 6% of the 239 samples analysed at levels ranging from 0.2 to 0.8?g/kg. Citrinin was detected in apple juice, black pepper, figs, oats amongst other food samples analysed. These levels are very low. Ergot alkaloids30. Ergot is the sclerotium of the fungus Claviceps purpurea, which infects wild grasses and cereals. The ergots produce a range of up to 40 different alkaloids and the six most prevalent are ergotamine, ergocornine, ergocristine, ergocryptine, ergosine and ergometrine along with their - inine stereoisomers. Typical symptoms of ergotism are gangrene and/or hallucinations and convulsions. At lower levels of contamination they can cause vasoconstriction and reproductive effects. 31. Commission Recommendation 154/2012 covers the monitoring of the presence of ergot alakloids in food and feed. The monitoring focuses on the following alkaloids and their inine forms: ergocristine/ergocristinine, ergotamine/ergotaminine, ergocryptine/ergocryptinine, ergometrine/ergometrinine, ergosine/ergosinine, and ergocornine/ergocorninine14. 32. A total of 122 samples of cereals and cereal based products were analysed for the above 12 alkaloids. Ergot alkaloids were detected in 12% of samples analysed with levels ranging from 2-21 ?g/kg. Again these levels are low and below the average values reported by EFSA5.Sterigmatocystin33. Sterigmatocystin is a mycotoxin that is produced by more than 50 fungal species, including Aspergillus Versicolor which is the most common source. Sterigmatocystin is commonly found in grains and grain-based products. It is a precursor of aflatoxin and is also carcinogenic, but less potent than aflatoxin.34. Sterigmatocystin was detected in 3% of the 200 samples analysed, at levels ranging from 0.2 to 0.7?g/kg. Sterigmatocystin was detected in ginger, chilli powder, nuts, turmeric and hot chilli powder. These results are low and well below the levels quoted in the EFSA opinion8.Fumonisins35. Fumonisins occur frequently in cereal grains, including maize. They are produced by Fusarium fungi, and the most significant fumonisins are FB1, FB2 and FB3. Fumonisins have been related to oesophageal cancer in humans, and to liver and kidney toxicity in animals. 36. In this survey, FB1 was detected in one sample of figs of the 111 samples analysed, at a level of 10?g/kg. This is much lower than average levels reported6.Alternaria toxins37. Alternaria toxins are mycotoxins produced by Alternaria species that cause plant diseases on many crops. Alternaria toxins have been reported to occur in oilseeds, olives, apples, citrus fruits and a number of other fruits and vegetables. This study measured levels of the alternaria toxins - alternariol (AOH), tenuazonic acid (TEA), alternariol monomethyl ether (AME), altenuene, altertoxin 1(ATX) and tentoxin (TEN). AOH and AME are considered as carcinogens, whereas AME, TEA and ATX are fetotoxic and teratogenic in rats. In addition, it has been suggested that in certain areas in China alternaria toxins might be responsible for oesophageal cancer. However there is generally a lack of toxicity data.38. Alternaria toxins were not detected in the 175 samples analysed. Conclusion 39. The results from this survey provide information to enable the FSA to obtain a picture of the levels of rarely tested for mycotoxins. In total, 400 samples were analysed for a range of mycotoxins, chosen on the basis of the commodity and the potential for its mycotoxin contamination. 40. Overall the levels of mycotoxins found in this survey were low. 41. With current knowledge and agricultural practices the provision of mycotoxin-free food samples is not possible, since the mycotoxins cannot be removed completely from the foods they are in. The FSA aims to establish and confirm that levels of contaminants and natural toxicants such as mycotoxins do not pose an unacceptable risk to human health and to ensure that they are within statutory limits where set. 42. The findings of this survey did not identify any specific food safety concerns for the general population from exposure to mycotoxins from these products. Abbreviations ARAnalytical ReagentCITCitrinin COSHHControl of Substances Hazardous to HealthEFSAEuropean Food Safety AuthorityHPLCHigh performance liquid chromatographyidInternal diameterLC/MS/MSLiquid chromatography/tandem mass spectrometryLODLimit of DetectionLOQLimit of QuantificationndNot Detectedppb or ?g/kgparts per billion or microgram/kilogramppm or ?g/gparts per million or microgram/gramPASPremier Analytical ServicesRSDRelative Standard DeviationSCFScientific Committee for FoodSMCSterigmatocystinTDITolerable Daily IntakeReferences 1Pitt, J.I. and Hocking, A.D. (1997), Fungi and Food Spoilage (1997). Blackie Academic Press, Sydney.2Samson, R.A., Hoekstra, E.S., Frisvad, J.C. and Filtenborg, O. (1996) Introduction to Food Borne Fungi. CBS, Delft, The Netherlands.3IARC (1993), Monographs on the Evaluation of Carcinogenic Risks to Humans. Volume 56 (Some Naturally Occurring Substances: Food Items and Constituents, Heterocyclic Aromatic Amines and Mycotoxins. IARC, Lyon, France. (2001), WHO Food Additives Series 47 FAO Food and Nutrition Paper 74. Safety Evaluation of Certain Mycotoxins in Food.5Scientific Opinion on Ergot alkaloids in food and feed 6Scientific Opinion on the risks for human and animal health related to the presence of modified forms of certain mycotoxins in food and feed and FAO/WHO (Food and Agriculture Organization of the United Nations/World Health Organization), 2012. Safety evaluation of certain food additives and contaminants. Fumonisins. WHO Food Additives Series, 65, 325 - 794.7Scientific Opinion on the risks for public and animal health related to the presence of citrinin in food and feed Opinion on the risk for public and animal health related to the presence of sterigmatocystin food and feed Opinion on the risks for animal and public health related to the presence of Alternaria toxins in feed and Food Standards Agency Regulation (EC) No.1881/2006, as amended()11Food Survey Information Sheet 04/10, Surveillance programme for mycotoxins in foods (Year 1: Cereals and cereal products)12 Food Survey Information Sheet 02/11, Surveillance programme for mycotoxins in foods (Year 2) Survey Information Sheet, Surveillance programme for mycotoxins (Year 3: Mycotoxins in ethnic foods) . Commission Recommendation 154/2012 on the monitoring of the presence of ergot alkaloids in feed and food information Food Standards Agency Aviation House 125 Kingsway London WC2B 6NH E-mail: ChemicalContaminants@foodstandards..ukAppendix 1, table 1: Sample Details SAMPLE CODEPRODUCT DESCRIPTIONBRANDUNIT SIZEUSE BY/BEST BEFORE DATEBATCH CODEDECLARED COUNTRY OF ORIGINRETAILER NAME13B-02406Ground black pepperSainsbury's250g14/10/20131287 BPortugalSainsbury's 13B-02407Whole black pepperMorrisons200gMAY 20153133None declaredMorrisons13B-02408Turmeric powderIndus400gSEP 20153177 - L2573None declaredTesco Extra13B-02409Haldi ground turmericRajah100g17 04 2015None declaredNone declaredSainsbury's 13B-02410Soft figs - ready to eatWhitworths175gJAN 2014L3092B 775 1None declaredMorrisons13B-02411Pear slices in fruit juiceAsdaDrained weight: 530gOCT 20132 124 1 JBS ZSouth AfricaAsda13B-02412Pear halves with juicePrincesDrained weight: 230gAPR 20153 095 4GB 6None declaredTesco Extra13B-02413Italian peeled plum tomatoes in tomato juiceAsda400gSEPT. 2014PIA1 LM236 PPItalyAsda13B-02414Pressed apple juiceInnocent900ml08/08/131 G 3175None declaredSainsbury's 13B-02415Apple & cherry pressed juiceMorrisons900ml04 SEP177WNetherlandsMorrisons13B-02416Cherry juice drinkCherry Good1 litre11 SEP 13X201 3174None declaredTesco Extra13B-02417Cherries & berries juiceAsda3 x 200mlNOV 13X302B 3151United KingdomAsda13B-02418Red grape juice - not from concentrateVitafit1 litre31 JUL 14X8 3151None declaredLidl13B-02419Spiced tomato juiceBig Tom75clFEB 15DNone declaredMorrisons13B-02420Frosted flakesCrownfield500g24.05.20147447095 144 NNone declaredLidl13B-02421Fruit loaded chunky granolaFuel400g08.06.2014161EEAAsda13B-02422Stay fresh wholemeal sliced bread - mediumTesco800g21 JULF33 191 0436United KingdomTesco Extra13B-02423Rye crispbreadFinn Crisp250g20 04 2014Production date:20 04 2013FinlandSainsbury's 13B-02424Green asparagus spearsKingfisherDrained weight:230gMAR 2017PZ.LB L3065PeruMorrisons13B-02425Red kidney beansHeinzDrained weight:220g05-20151413 FCEEATesco Extra13B-02426Soya beansTesco500gMAY 2014Display until FEB 2014L3144-2BelgiumTesco Extra13B-02427Pitted black Spanish olivesFragataDrained weight:380gMAY 20153133SpainMorrisons13B-02428Pitted black olives in brineCrespoDrained weight:380g15/04/16SQ R14 L1 105 U34332343353433634338MoroccoSainsbury's 13B-02429Pinot grigio 2012 Delle VeneziePalastri Italia75clNone declaredL3156 0816L12596082CItalySainsbury's 13B-02430Garnacha rosé 2012Gran Familia Las Primas75clNone declaredL-2113216VSpainTesco Extra13B-02431California merlotOak Leaf75clNone declaredL13112V BUnited StatesAsda13B-02432Cherry wineCherry B4 x 113mlNone declaredL3079/3None declaredAsda13B-02433Wheat beerErdinger50cl04-2014L111304None declaredMorrisons13B-02434Weissbier - wheat beerFranziskaner500ml05.2014L127316None declaredLidl13B-02435Belgian wheat beerHoegaarden75cl12.05.143.2None declaredAsda13B-02436Cloudy wheat beerWeihenstephan500ml05.06.14None declaredNone declaredTesco Extra13B-02437Non-alcoholic wheat beerBavaria N.V.6 x 33cl07-2014None declaredNone declaredMorrisons13B-02438Pure sunflower oilFlora1 litreMAY 14128None declaredMorrisons13B-02439Organic sunflower oilPura500mlMAY 2014L3136 1None declaredTesco Extra13B-02440Sunflower seedsTesco300gJUN 2014L3161B 930 1United StatesTesco Extra13B-02441Monkey nutsCofresh450g24/MAY/14L2/149United KingdomTesco Extra13B-02442Organic whole milkYeo Organic1 litre19 JULM3None declaredTesco Extra13B-02443Filtered skimmed milkTesco Pure2 litres01 AUGF72114PRO14H5/R2/S4124616-12085United KingdomTesco Extra13B-02444Red seedless grapes - "flame"Asda500g26 JULNML14ABatch: 549432Site: 903129EgyptAsda13B-02445Seedless green grapesTesco500g26 JULGRVariety: SugroneEgyptTesco Extra13B-02446Baby San Marzano tomatoesMorrisons250g27 JUL0522/01 L6Class 1United KingdomMorrisons13B-02447Ready-to-eat pears - "Packhams"Morrisons4 pears26 JUL2556/EW265 - 70mmClass 1United KingdomMorrisons13B-02448Red grape juice - not from concentrateTropicana1 litre17/08/13H 26UD 22BINone declaredTesco Extra13B-02449Asparagus bundleTesco250g26 JULWD03PeruTesco Extra13B-02450Semi-skimmed milkAsda568ml03 AUGBMF WD034 L2(1)United KingdomAsda13B-02451Ground black pepperTesco Everyday Value100gJUN 20153153None declaredTesco Extra13B-02452Ready-to-eat soft figsMorrisons Wholefoods600gNOV 2013L3151N 765 1TurkeyMorrisons13B-02453Garland figsAsda Wholefoods250gMAY 2014350020518-02-7513116/001TurkeyAsda13B-02454Plain flourBe-Ro500gMAR 20143155 RLUnited KingdomAsda13B-02455Medium oatmeal - stonegroundMornflake500g05 2014L3140 P8None declaredMorrisons13B-02456Pure original Basmati riceTilda500gJUN 2015L4 13162P: 01-06-2013E: 01-06-2015None declaredTesco Extra13B-02457Long grain riceAmira1kgFEB-2015MFD 3/2013B.N. 272795IndiaMorrisons13B-02458MacaroniMarshalls Pasta500g01/2015L130190 0514EEAMorrisons13B-02459Cous cousAsda500gJUN 201462 GB 3163United KingdomAsda13B-02460Pearl barleyGreat Scot500gAPR 2014L3120A 855 2None declaredTesco Extra13B-02461Kidney beansTesco Wholefoods500gMAY 2014L3150B 870 2ChinaTesco Extra13B-02462Soya beansMorrisons Wholefoods500gMAR 2014L3080A8121None declaredMorrisons13B-02463Organic almondsTesco Organic200gNOV 2013L3004006 BN01ItalyTesco Extra13B-02464Dried skimmed milkAsda340gNOV 20143136United KingdomAsda13B-02465Green seedless grapesTOP500gNone declaredClass 1 Variety: SugroneCode 530SpainSpar13B-02466Blush pearsCape800gNone declaredNone declaredSouth AfricaSupervalu13B-02467TomatoesSeason Harvest5'sNone declaredClass 1HollandCostcutter13B-02468Plain breadSunblest800g04 AUGBE63209 1810United KingdomNisa Extra13B-02469Burger buns (6)Quickbury300g21.10.13W52GermanyCentra13B-02470Fresh butter milkDale Farm568ml08 AUG0United KingdomNisa Extra13B-02471Italian peeled plum tomatoes in tomato juiceEpicure400gDECEMBER 2014FARU5 P L E259ItalySupervalu13B-02472Passata with basilNapolina390gOCT.2014PIA1 LM286 BAItalySpar13B-02473Apple juice (made from concentrate)Centra1 litreJAN 1421813A10None declaredGormley's Centra13B-02474Irish muesliLifeforce750g09/04/2014None declaredNone declaredGormley's Centra13B-02475Toasted rice cerealSupervalu Rice Krunchies440g27 FEB 201431470953None declaredSupervalu13B-02476CornflourBrown & Polson250g02/2015L3050None declaredDay Today13B-02477Soda breadMortons Flour1.5kg28 FEB 2014L28 D:13 1912None declaredNisa Extra13B-02478Speedicook porridge oatsWhite's Speedicook750g22 APR 143 112None declaredCentra13B-02479Express egg fried riceCentra250gAPR 20143GE2ANone declaredGormley's Centra13B-02480Arborio risotto riceGallo Gran 500g02/07/2015None declaredNone declaredGormley's Centra13B-02481Organic wholegrain spaghettiBunalun Organic500g06/11/2014L2452 3433None declaredSpar13B-02482Condensed milkNestlé Carnation397g07-2014L30240294M0None declaredCostcutter13B-02483Red split lentilsBuchanans500gFEB 1413011None declaredCentra13B-02484Cooked white riceRoss1kgMAR 20153077FK L5EEAGormley's Centra13B-02485Cherry juice drinkAsda1 litre22/OCT/201377 (Su20) BNDSpainAsda13B-02486Cherry juice drinkWaitrose1 litre02 OCTDisplay until 30 SEP215SpainWaitrose13B-02487Cherry juice drinkSainsbury's1 litre22.10.1313SpainSainsbury's 13B-02488Sour cherry nectar (from concentrate)Dimes1 litre14.05.2014PNO: 1405-IZ M6TurkeyAsda13B-02489Pressed red grape juiceWaitrose1 litre01 FEB 14X307 3213United KingdomWaitrose13B-02490Purple grape juice (from concentrate)Welch's750ml25 SEP 133208 K204 BNone declaredSainsbury's 13B-02491Organic tomato pasteTarantella Organic300g11/2014PU7 M319 2-None declaredAsda13B-02492Triple strength tomato puréeBomba!200gDEC 2014LM 342ItalyWaitrose13B-02493Sundried tomato pasteWaitrose Cooks' Ingredients180gMAY 2016LH 144ItalyWaitrose13B-02494FigsSainsbury's500gAPR 2014L3190B 770 1TurkeySainsbury's 13B-02495Fig preserveMammy Jamia's340g06.2015L3156 0816United KingdomWaitrose13B-02496Pressed apple juiceDon Simon1 litreAPR 2014L-3106 12 BSPUnknownAsda13B-02497Pressed white grape juiceAsda1 litreJAN 14X308 3193United KingdomAsda13B-02498Whole grain wheat cereal Nestlé Shredded Wheat30 biscuits30.04.201431980952 GNone declaredSainsbury's 13B-02499Rye crispbreadAsda Good For You200g28.11.2014None declaredFinlandAsda13B-02500Organic stoneground 100% wholemeal flourMaud Foster Mill1.5kg12 DEC 13None declaredNone declaredSyston Park Farm13B-02501Organic Scottish oatmealRude Health The Oatmeal750g20.05.2014L13140TOUnited KingdomWaitrose13B-02502Oat drinkProvitamil1 litre28/06/14PROD: 28/06/13Produce of several countriesAsda13B-02503Organic porridgeJordans750g07 01 20153189 FUnited KingdomAsda13B-02504Red camargue & wild riceWaitrose Love Life500gMAY 20143128 FS VP(2)Produce of several countriesWaitrose13B-02505Basmati brown riceAsda1kgJAN 20153204 MCRNone declaredAsda13B-02506Oats 'n' bran bread flourWessex Mill1.5kg17 JUN 20140816956CanadaGermanyFour Seasons Farm Shop13B-02507Wholemeal bread mixSainsbury's500gDEC 20133151United KingdomSainsbury's 13B-02508Pearl barleyWaitrose Love Life500gJUL 20143189CUnited KingdomWaitrose13B-02509Rye flourAsda1kgNOV 20133165 F4XUnited KingdomAsda13B-02510Asparagus spearsAsda250g17 OCT 2014None declaredUnited KingdomAsda13B-02511Red kidney beansWaitrose Love Life500gAPR 20143100BChinaWaitrose13B-02512Suffolk Blonde wheat beerSainsbury's Taste The Difference500ml24 JUL 14None declaredUnited KingdomSainsbury's 13B-02513Golden wheat beerSleaford Brewery500ml12.13None declaredUnited KingdomFour Seasons Farm Shop13B-02514Three grain strong beerTripel Karmeliet33cl15/05/15None declaredBelgiumWaitrose13B-02515Bavarian dunkel weissbier - dark wheat beerWaitrose500mlFEB 2014L13059GermanyWaitrose13B-02516Sunflower oilAsda1 litreJUL 2014H183Produce of several countriesAsda13B-02517Sunflower oilSainsbury's1 litreJUL 2014H184EEASainsbury's 13B-02518Sunflower oilWaitrose Essential500ml30/09/2014L+3176None declaredWaitrose13B-02519Original salted peanutsKP300g07 12 133210MC8A RUnited KingdomAsda13B-02520Cashew nutsWaitrose Love Life400g27/01/14275AT/30200 15BrazilWaitrose13B-02521Puy lentilsMerchant Gourmet500g04.04.16None declaredFranceWaitrose13B-02522Dark rye crispbreadMorrisons200g13 06 14None declaredFinlandMorrisons13B-02523All bran originalKellogg's750g23/03/14L1None declaredMorrisons13B-02524Sunflower oilMorrisons1 litreJUL 2014H197United KingdomMorrisons13B-02525Sunflower oilBorges1 litre24/07/2015L: 106633PRD: 24/07/2013SpainTesco13B-02526Milk powderEast End250g31/12/2013RW12339EEAMorrisons13B-02527Red kidney beansMorrisons Wholefoods500gJUN 2014L3163A870 1Produce of several countriesMorrisons13B-02528Red kidney beans in salted waterKTCDrained weight: 240g31/12/2015PG1LH190 RK OFNone declaredSainsbury's 13B-02529Whole figs in syrupMorrisonsDrained weight: 210g30.09.2014L 111/215ESpainMorrisons13B-02530Pearl barleyMorrisons Wholefoods500gJUN 2014L3170A8123United KingdomMorrisons13B-02531Easy cook pre-fluffed riceSea Isle5kgAPR 201516042013Produce of several countriesMorrisons13B-02532Superior aged Basmati riceBadshah5kgJUN 2015BA 3178IndiaSainsbury's 13B-02533SemolinaCypressa500gAUG 201413192None declaredMorrisons13B-02534Greek black olivesFOSDrained weight: 215g30/07/2015LN087130403J01GreeceTesco13B-02535Shiraz-Malbec 2011J. P. Chenet750ml?L20131201067515/067519No: 078296 & 078300FranceMorrisons13B-02536Prepared lentilsD'aucyDrained weight: 265g31 05 20186420 L:H 2F 3 038-BEEAMorrisons13B-02537Small lentilsЗa?cpa500g31/12/2014L.130729 009None declaredTesco13B-02538Red lentilsGama500g08.05.2014L130508TurkeyMorrisons13B-02539Urid dal whiteKTC500gMAR 2015GRN 1457 N613031PProduce of several countriesMorrisons13B-02540Organic green lentilsCrazy Jack Organic250gDec 2014Lot 3166 C3None declaredSainsbury's 13B-02541Whole British milkSainsbury's568ml28 OCTDG001M D1United KingdomSainsbury's 13B-02542Linguine fresh egg pastaTesco350g12 NOVLA 3TJ2ItalyTesco Extra13B-02543Self raising wholemeal flourAllinson1kgFEB 2014F4X 3242None declaredSainsbury's 13B-02544Wholemeal medium sliced breadHovis800g23 OCTX86D F PNone declaredSainsbury's 13B-02545Organic seedles red grapesSainsbury's So Organic400g23 Oct00166E Grown by A TarulliVariety CrimsonItalySainsbury's 13B-02546Pressed tomato juiceSainsbury's1 litre17.11.1313SpainSainsbury's 13B-02547Spicy tomato juiceDel Monte Occasions1 litreJAN 14X307 3202United KingdomTesco Extra13B-02548Tangy tomato juicePrinces1 litreMAR 2014S L3227C AUnited KingdomTesco Extra13B-02549Strong brown flourTesco1.5kgAPR 2014F3X 3290United KingdomTesco Extra13B-02550Crusty wholemeal bread mixTesco500g11 APR 14GWB 3284United KingdomTesco Extra13B-02551Honey coated wholegrain wheat, corn and oat cerealTesco Multigrain Boulders375g31 MAY 20143247083800C1C2C3FranceTesco Extra13B-02552Belgian wheat beerTesco Finest750ml05/15L13-13122BelgiumTesco Extra13B-02553Organic wholegrain rye flourDoves Farm Organic1kg18/06/14JC3261Produce of several countriesTesco Extra13B-02554Ready to eat figsTesco250gJUN 2014L3269A7752TurkeyTesco Extra13B-02555Unfiltered North American craft wheat beerBlue Moon355ml30 JUN 14L3224 MNone declaredTesco Extra13B-02556Tomato juice made from concentrateTesco1 litreJUN 14X6 3261United KingdomTesco Extra13B-02557Mixed fruit juice drinkCherry Vimto1 litreJUL 2014Q L3192C CNone declaredTesco Extra13B-02558Cherry tomatoes in rich tomato sauceTesco Finest400g07/2014LM211 PN10 FD3ItalyTesco Extra13B-02559Mixed nutsSainsbury's300gJUL 201444 T 3247Produce of several countriesSainsbury's 13B-02560Wholewheat penneSainsbury's500gAug 2015L3215DItalySainsbury's 13B-02561Vegetable juiceV81 litre19.09.2014C LH200None declaredTesco Extra13B-02562Ready oatsSainsbury's500g26/09/20143269 1United KingdomSainsbury's 13B-02563Cloudy pressed apple juiceCawston Press250mlSEP 2014L3157 RD5United KingdomTesco Extra13B-02564OatbranTesco500g10 2014L3277 P8United KingdomTesco Extra13B-02565 English apple juice - Ida Red, mediumDuskin1 litre6 FEB 20151848United KingdomHaguelands Farm Shop13B-02566Chopped tomatoes in tomato juiceSainsbury's Basics400g03.2015BLF1 LM 268 CItalySainsbury's 13B-02567Pear halves in light syrupDel MonteDrained weight: 230g30.06.201513I12 BBH 2 SL S ZNSouth AfricaSainsbury's 13B-02568Dornfelder light red wineBiddenden Gribble Bridge750mlNone declaredNone declaredUnited KingdomHaguelands Farm Shop13B-02569Sweet breadHeavenly Bread800g16 11-13None declaredNone declaredCostcutter13B-02570Roasted sunflower seedsMeray320g24/06/2014LOT/M: 2013.143 SKT/MHDProd-Dat 24/06/2013None declaredSt James Supermarket13B-02571Pearl barleyCo-Op Wholefoods500gSEP 201462 AH 3260United KingdomCo-op13B-02572Brown riceHeritage500gMAR 2015VT 3 074 VP(2)UnknownCostcutter13B-02573Tomato paste double concentrationKyknos410g09/2014LM 205GreeceSt James Supermarket13B-02574Pure premium tomato juiceBBB1 litre31 JUL 2014L054EEASt James Supermarket13B-02575Black Gemlik olivesDurmaz800g01/02/201522/26/01_1_1_3.2Verpackungs datum 01/02/2013TurkeySt James Supermarket13B-02576Dehydrated black olives - kuru seleMarmarabirlik800g26/06/2014P:3-1TurkeySt James Supermarket13B-02577Large seeded loafGregg's800gNone declaredNone declaredNone declaredGregg's13B-02578Buckwheat flourDoves Farm 1kg27/06/14JC3270Produce of several countriesWaitrose13B-02579Ground black pepperKania Spices50g2017L3225ADNone declaredLidl13B-02580Multigrain hoopsGreat Start375g04 06 2014L100464997PolandCo-op13B-02581Organic rye flourBacheldre Watermill1.5kg22/06/143296 0847None declaredWaitrose13B-02582Scottish oatcakesMcAllisters300g30 06 14P262BUnited KingdomLidl13B-02583Organic dried figsWaitrose Organic250g30/01/2014L 132690210Supplier: 207DFFTurkeyWaitrose13B-02584Kalamata olivesWaitrose220g14 DECDisplay until 12 DECItalyWaitrose13B-02585Sunflower seedsWaitrose150gOCT 2014L3280A 930 1United StatesWaitrose13B-02586Pearl barleyCommunity Foods500gOct 20143295 C3United KingdomCo-op13B-02587Yellow split peasMontedos Wholefoods500gOCT 2015131021-BN0023PROD: OCT 2013None declaredLidl13B-02588Ground black pepperStonemill100gSEP 20153256None declaredAldi13B-02589Crusty wholemeal bread mixThe Pantry500g29 APR 14GWB 3302None declaredAldi13B-02590Golden puffs (puffed wheat)Harvest Morn375g31 OCT 14282 C 9None declaredAldi13B-02591Wholemeal rye crispbreadSavour Bakes250g04.08.2014L13300C/1None declaredAldi13B-02592Tomato juice from concentrateMorrison Savers1 litreAPR 2014X L3283C BUnited KingdomMorrison's13B-02593Sunflower oilSolesta1 litre28/03/2015LE3283None declaredAldi13B-02594Ground black pepperEast End1kgMAR 20142074 L8None declaredRahim Brothers13B-02595Turmeric powderRadhuni400g01 AUG 201412080046BangladeshRahim Brothers13B-02596Fennel seedsNatco1kgJUL 2015Prod: JUL 2013Batch: 130724-BN0003None declaredRahim Brothers13B-02597ChestnutsTesco2kgNone declaredNone declaredItalyTesco13B-02598Baker's Blend Sharpham Park1kg10 APR 14None declaredNone declaredWaitrose13B-02599Dark rye crispbreadRyvita250g08.09.20141 3312None declaredTesco13B-02600Tomato juice (not from concentrate)Sunraysia750ml28 03 15HCFranceWaitrose13B-02601? La Grecque olivesTescoDrained weight: 220gSEP 20153268SpainTesco13B-02602Soya minceTesco Wholefoods375gAUG 2014L3308A8122SerbiaTesco13B-02603Wheat branShire Foods500gJun 14WHE500/173102United KingdomDents of Hilgay13B-0260450/50 white bread Kingsmill800g17 DECSH05 3 345 1132United KingdomIceland13B-02605OatcakesBramble House200g15.01.14None declaredNone declaredDents of Hilgay13B-02606Avi?iniai biscuitsHome Foods350g15-02-2014None declaredNone declaredLituanica13B-02607Garlic and coriander naansCurrymate240g02 MAR 14None declaredNone declaredFarmfoods13B-02608Roasted and salted pistachiosMarks & Spencer150g28/02/2014L3039036United StatesMarks & Spencer13B-02609Organic soft figs Crazy Jack Organic250gDEC 20143262 lot 2-1159TurkeyBudgens13B-02610Mixed seed bread mixJames Martin Bakery500gAUG 20143309 LM L4United KingdomAsda13B-02611100% pure sunflower oilGoldenfields2 litres30/11/2014L+3317None declaredIceland13B-02612Sunflower oilSuperValu1 litre01 2015L13277A1None declaredBudgens13B-02613Soya milk - sweetenedMarks & Spencer1 litre28 12 2013F33170United KingdomMarks & Spencer13B-02614Soya milk - unsweetenedAsda1 litre02/01/14V4827 30/12/13United KingdomAsda13B-02615Whole milkYorkshire Local2 litres18 DECEZUnited KingdomLituanica13B-02616Pressed apple juiceSuperValu1 litre10 APR 14L3MDisplay until 7 APR 14None declaredBudgens13B-02617Layer figsDemos250gJuly 20144029090021053-11-315TurkeyDents of Hilgay13B-02618Tomato juiceSunpride1 litreNOV 14X2 3306None declaredBudgens13B-02619Sweet Worcester pressed apple juiceWatergull Orchards750ml20 09 14None declaredUnited KingdomDents of Hilgay13B-02620Apple juice (from concentrate)Marks & Spencer3 x 200ml09 03 20143301CUnited KingdomMarks & Spencer13B-02621Pressed Bramley apple juiceSandringham Apple Juice750ml31/12/14L284United KingdomBudgens13B-02622Grape nectar (from concentrate)Cido1 litre26.10.1427.10.13None declaredLituanica13B-02623Whole black peppercorns Ko Spice50gAUG 201528/SEP/2013IndiaIceland13B-02624Fennel seedsTRS100g31/10/2015P131016IndiaSpice Market13B-02625Turmeric powderTRS100g31-10-2015P131028IndiaSpice Market13B-02626Ground riceWhitworths500gOCT 2014L3275A8002United KingdomBudgens13B-02627Viso grüdo (wholemeal rye flour)Malsena1.75kg28 08 201401 13 H 2912None declaredLituanica13B-02628British porridge oatsMarks & Spencer500g10/20143301United KingdomMarks & Spencer13B-02629SpaghettiCasa Buona1kg11/2016L3310MItalyFarmfoods13B-02630FusilliDelverde500g20.09.2015L 238115 265PROD: 20.09.2012None declaredBudgens13B-02631CouscousAtlas1kg26/04/15P. 26/04/13MoroccoSpice Market13B-02632Mie?in?s kruopos (barley groats)S & S800g04102014None declaredLithuaniaLituanica13B-02633BuckwheatLimor800g11112014K1LithuaniaLituanica13B-02634Buckwheat flakesGalinta500g22.10.2014None declaredLithuaniaLituanica13B-02635Red kidney beansKerala1kg30/12/2015RB30/2013Mfg Date: 30/05/2013None declaredSpice Market13B-02636Organic red kidney beans in waterAsdaDrained weight: 240gSEP 2017W OR1Z 3273 01United KingdomAsda13B-02637Red kidney beans in waterBatchelorsDrained weight: 240gOCT 2017W H5RW 3296 01None declaredBudgens13B-02638Red kidney beans in salted waterDunn's RiverDrained weight: 230g31/12/2015V1 H250 RK TNone declaredSpice Market13B-02639Blend of water and soya beansSoya Soleil1 litre02/09/2014U3608EEABudgens13B-02640Green lentils in waterAsdaDrained weight: 265gSEP 2017W R9ZW 3245 08United KingdomAsda13B-02641Strong wholemeal flourMarriage's1.5kgMAR 201413268 36125None declaredBudgens13B-02642Figs in light syrupAsdaDrained weight: 210g30.09.2015L111/241 ESpainAsda13B-02643Cabernet sauvignon 2011Wolf Blass Yellow Label750mlNone declaredL22492Z21 W3AD5122130947AustraliaMace,Lavender Hill Services13B-02644Nettle wineLyme Bay Winery750mlNone declaredV 0028956V 0028943None declaredDents of Hilgay13B-02645Hojiblanca pitted black olivesHeliopolisDrained weight: 340g08.2016L3263-07SpainAsda13B-02646Sour cherry nectar (from concentrate)Golden Gate1 litre05.06.14#5GermanyBounds Green Supermarket13B-02647White grape juice (pressed)Stute1 litre30.06.15/05 M19/1None declaredBounds Green Supermarket13B-02648Organic soya drinkAlpro1 litre15/02/14V0208EEASainsbury's 13B-02649Soyabean curd - firmMoringa349g04 10 2014BUnited StatesSainsbury's 13B-02650Extra salted sunflower seedsTadim200g11.11.2014A7 L1193315PRODUCTION DATE 11.11.2013TurkeyNewspoint Newsagent13B-02651Sunflower seedsSainsbury's100gDEC 2014L3340A 900 1United StatesSainsbury's 13B-02652Roasted and salted sunflower seedsBaktat150g04.2014L.D 119TurkeyBounds Green Supermarket13B-02653Jersey full cream milkGraham's Gold1 litre26 JANNone declaredUnited KingdomSainsbury's 13B-02654Sushi riceYutaka500g251116None declaredNone declaredSainsbury's 13B-02655Organic whole wheat cerealWeetabix 24 biscuits30/11/201413334 2United KingdomSainsbury's 14B-00173Green lentilNatco500gDEC 2015131202-BN0007PROD: DEC 2013None declaredSainsbury's 14B-00174Poivre noir mouluMedia Food100g2016Lot 131025None declaredMediterranean Boucheriere14B-00175Black pepper powderTRS400gJAN 2015BPP 13020IndiaAsian Foodstore14B-00176Green cardamomTRS200g31-08-2015P130812GuatemalaMadina Stores14B-00177Pearl barleyJCR500g31/08/2015None declaredNone declaredAlbarka14B-00178Pitted black olives in brineSiof2000g08/09/2015SY 252 F CAL 30/33(1)MoroccoAlbarka14B-00179WalnutsKB Natural Foods140gJUN 15HZ 021213United StatesMadina Stores14B-00180Ground almondsLoubnan Natural Foods200g08/11/1441356None declaredAlbarka14B-00181Cardamon teaAhmad Tea500g01/05/2015Packing date: 01/05/2012Sri LankaAlbarka14B-00182Sunflower blackLoubnan Natural Foods200g12/10/14None declaredNone declaredAlbarka14B-00183Soya wadiJCR200g31/12/2014None declaredNone declaredAsian Foodstore14B-00184Soya beansTop Op500gDEC 2014N/00402792/121211 Grn 955IndiaAsian Foodstore14B-00185Soya minceTRS250gMAR. 2015L13109IndiaAsian Foodstore14B-00186Red kidney beansNatco500gSEP-2015130903-BN0016Prod: SEP-2013ChinaAsian Foodstore14B-00187Sliced black olivesFigaroDrained weight: 480g04/07/201601L185013 HRNPRD: 04/07/2013SpainMediterranean Boucheriere14B-00188Organic skimmed milkDuchy Originals1.136 litres25 FEBM1United KingdomWaitrose14B-00189Cloudy apple juiceCopella750ml14/03/14CAUUnited KingdomWaitrose14B-00190Cherry juice drinkMarks & Spencer1 litre28/02/14364UDISPLAY UNTIL 24/02/14SpainMarks & Spencer14B-00191Pure grape & raspberry juiceMarks & Spencer1 litre28/03/14S2 DISPLAY UNTIL 24/03/14United KingdomMarks & Spencer14B-00192Asparagus spearsSainsbury's420g21 FebB0090LGrown by Altar, MexicoMexicoSainsbury's 14B-00193Bunched asparagusWaitrose450gNone declared111ALNDISPLAY UNTIL 21 FEBMexicoWaitrose14B-00194British Conference pearsTescoBag of 521 FEBGrown by: Robert Littlechild60/65mm SC:SGT03 B13United KingdomTesco14B-00195Perfectly ripe green William pearsMarks & SpencerPack of 4None declaredDISPLAY UNTIL 21/02/14B L1 450865/70mmItalyMarks & Spencer14B-00196PearsWaitrose EssentialBag of 7None declaredDisplay until: 27 FEBSUPPLIER 183LLXCommodity code: 613640PortugalWaitrose14B-00197Loose red grapesMarks & SpencerRandom weight bagsNone declaredCrimson (point of sale notice)None declaredMarks & Spencer14B-00198Black seedless grapesWaitrose Essential500gNone declaredDISPLAY UNTIL 21 FEBVariety Midnight BeautySupplier 331DBLSouth AfricaWaitrose14B-00199Fresh tagliatelleMarks & Spencer400g06/03/2014L 3 404DJItalyMarks & Spencer14B-00200Organic rye rossiskyThe Village Bakery Melmerby800g22 FEBDUnited KingdomWaitrose14B-00201Mulit-seed & cereal pittasThe Food DoctorPack of 607 MAR 14None declaredUnited KingdomWaitrose14B-00202High bran sliced loafMarks & Spencer400g21/02/20144SB02 A GUnited KingdomMarks & Spencer14B-00203CrispbreadMarks & Spencer125g05/11/14None declaredGermanyMarks & Spencer14B-00204Mixed seed crispbreadJacob's5 packs of 430 08 14SP5 3352UnknownWaitrose14B-00205Organic Emmental cheese & pumpkin seed crispbreadDr. Karg's200g13/JUL/2014BKKA3-342134GermanyWaitrose14B-00206Pearl barleyMarks & Spencer500g11/2014L3317A8703United KingdomMarks & Spencer14B-00207Barley flakesNeal's Yard Wholefoods500gJan 2015L4007UnknownHolland & Barrett14B-00208Whole grain rye breadSchneider Brot500g19.03A2GermanyWaitrose14B-00209Organic rye flourMarks & Spencer1kg31/03/2014JC3164United KingdomMarks & Spencer14B-00210Dark rye flourWaitrose1kg10/05/201413315 36598Produce of several countriesWaitrose14B-00211Whole Brazil nutsNeal's Yard Wholefoods500gOCT 1414037 2 80118BoliviaHolland & Barrett14B-00212Roasted salted macadamia nutsWaitrose100g10 MAY 1444 T 3353Produce of several countriesWaitrose14B-00213Fruit & fibreMarks & Spencer500g09/20143353 L7United KingdomMarks & Spencer14B-00214Spelt flourWaitrose1kg16/06/201413352 36969Produce of several countriesWaitrose14B-00215OatbranPrewett's400gAPR 2014RW13092United KingdomHolland & Barrett14B-00216ChickpeasMarks & SpencerDrained weight: 240g10/2017W 3295 R4MS 01United KingdomMarks & Spencer14B-00217Peach Garden Chardonnay 2012Marks & Spencer75clNone declaredL 3226 120306BulgariaMarks & Spencer14B-00218Shiraz & Mourvède 2013Fire Flower750mlNone declaredL0FD138741 3 204South AfricaWaitrose14B-00219Hulled sunflower seedsNeal's Yard Wholefoods500gOCT 1413345 2 79353United KingdomHolland & Barrett14B-00220Sweet' white sorghum flourBob's Red Mill500g19/03/2015156610 0537 19/09/2013United Stateshealthysupplies.co.uk14B-00221Fennel seedsKTC1kgDEC 20141FE WONT 130016None declaredHoo Hing14B-00222Coarse black pepperRajah400g02 10 2015None declaredNone declaredHoo Hing14B-00223Ground black pepperMillstone600gDec 2015176825Produce of several countriesAsda14B-00224Dried cardamom seedsWah Loong Co. Ltd113g30 MAY 20141003781ChinaHoo Hing14B-00225Turmeric powderKTC5kg3011201552131125None declaredHoo Hing14B-00226Black pepper groundSun Brand400g30 AUG 2014None declaredMalaysiaHoo Hing14B-00227Cherry apple drinkTymbark2 litres11.20143242358 A2PolandAsda14B-00228Dried barley (pudding)Jin Shin Foods200g30/08/2014None declaredChinaHoo Hing14B-00229Pink peanutsHoo Hing Ltd500g31/12/14Code: 10083ChinaHoo Hing14B-00230Juwar flourJalpur1kg30JUN 14L13361 JM L13345/VP3None declaredtheasiancookshop.co.uk14B-00231Fresh whole milkCo-Op568ml24 MARD31112 PR014United KingdomCo-op14B-00232Wholemeal sliced breadBrace's Classic800g22 MARG 58 U 4UnknownCo-op14B-00233Conference pearsMunday & JonesEachNone declaredNone declaredUnited KingdomMunday & Jones14B-00234Red grapesMunday & JonesApproximately 600gNone declaredNone declaredSouth AfricaMunday & Jones14B-00235Tomato juice (from concentrate)Co-Op1 litreAUG 2014WL 4044C CEuropean UnionCo-op14B-00236Malted brown bread mixCo-Op500g04AUG14GWB 4035United KingdomCo-op14B-00237Organic light rye 997 wholemeal flourShipton Mill1kg30 JUL 143333United KingdomWyedean Healthfoods14B-00238Rolled buckwheat flakesWyedean Healthfoods500g02/15None declaredNone declaredWyedean Healthfoods14B-00239Sunflower seedsQueenswood 250gDEC 2014L0224ChinaMunday & Jones14B-00240Organic sunflower seedsWyedean Healthfoods500gDEC 201410314 ORGANICChinaWyedean Healthfoods14B-00241Organic 100% wholemeal flourShipton Mill2.5kg30 AUG 1423670None declaredWyedean Healthfoods14B-00242Organic rye flakesWyedean Healthfoods500gOCT 201410304 ORGANICAustriaWyedean Healthfoods14B-00243Riesling 2012Devil's Rock750mlNone declaredA.P.Nr. 4 342 352 070 13L-13295WTGermanyCo-op14B-00244Biodynamic apple juiceOaklands Park Garden750cl22 OCT 201516B2None declaredWyedean Healthfoods14B-00245Medium sliced brown loafMorrison Savers720g29 MARRWF 3 GF 57None declaredMorrison's14B-00246Seedless green grapesMorrisonsRandom weight bagsNone declaredNone declaredChileMorrison's14B-00247Black cardamomsEast End150gAUG 20153 220L4None declaredThe Meat Centre14B-00248Ground turmericEast End400gFEB 20164 042 L6IndiaThe Meat Centre14B-00249Fennel seedsEast End375gDEC 20153 361 L3None declaredThe Meat Centre14B-00250Dry roasted peanutsMorrison Savers200g31 Aug 14115731 05814 AJ TH1NUT2ANone declaredMorrison's14B-00251Asparagus Morrisons150g18 APR0589/2 PeruMorrison's14B-00252Red globe seeded grapesPedregalsaBagNone declaredNone declaredPeruBilal Supermarket14B-00253Pitted black olivesKvuzat YavneDrained weight: 275g02.2016YA-311 13-036 LV(1201171521 on bottom)IsraelMorrison's14B-00254White bread mixVictoria Foods375gNOV 2014L9 4 059 LMNone declaredMorrison's14B-00255Cardamom blackIndus 150gAUG 20164017-L4384None declaredTesco14B-00256Wholewheat crispbreadProvita250g15 09 2014MAN 16 09 2013South AfricaTesco14B-00257Fada (cracked wheat)TRS1kg20/March/201513/110IndiaBilal Supermarket14B-00258Fennel seedsIndus 300gOCT 20153298-L1855None declaredTesco14B-00259Strong wholemeal bread flourWright's1.5kg26 SEP 1416151GWA4086United KingdomTesco14B-00260Self raising flourHomepride1kgMAR 20154036 GANone declaredMorrison's14B-00261Steamed wheat flourSuryaa1kg28 FEB 2017140205AIndiaLondis14B-00262Red grape & berries pressed juiceMorrisons1 litre13 JUN094 ZNone declaredMorrison's14B-00263Pressed red grape, raspberry and cherry juiceTesco1 litre28 MAY083RSpainTesco14B-00264Concord grape juiceKedem650ml070715A14MUnited StatesMorrison's14B-00265Walnut halvesGolden Tree175g31 Mar 2015413001KUnited StatesMorrison's14B-00266Black pepper cashewsGinco150gFEB 15R14028None declaredLondis14B-00267Juwar flourTRS1kg12/Sept/201513/285IndiaLondis14B-00268Sunflower seedsBodrum200g30.11.14None declaredSpainBilal Supermarket14B-00269Bunched asparagusElveden EstateBundleNone declaredNone declaredUnited KingdomElveden Estate Farm Shop14B-00270Almond alternative to dairy milkTesco Free From1 litre25 07 14H T039 T068 146 4 PF738743FranceTesco14B-00271Sliced seeded gluten free breadWarburtons Newburn Bakehouse600g23 JUNAKYRW ANFZ19None declaredTesco14B-00272All butter triple chocolate cookies - gluten freeTesco Finest150gNOV 144142BUnited KingdomTesco14B-00273Loose teaPG Tips250g09.2015L4112 2A620None declaredSainsbury's 14B-00274Assam tea bags - 100Tesco Finest250g SEP 2015L4153 9AIndiaTesco14B-00275Earl Grey tea bagsTwinings250g (100 bags)MAY 2016132 0000016152 UKNone declaredTesco14B-00276Jumbo raisins - partially rehydratedWhitworths325gDEC 2014L4153 B745 1Produce of several countriesTesco14B-00277aFairtrade green tea - 80 teabagsSainsbury's200gAUG 20154043None declaredSainsbury's 14B-00277bFairtrade green tea - 80 teabagsSainsbury's200gSEP 20154078None declaredSainsbury's 14B-00277cFairtrade green tea - 80 teabagsSainsbury's200gOCT 20154105None declaredSainsbury's 14B-00278aPure green teaTwinings200gAPR 201612 0000015216 UK 105China & AsiaSainsbury's 14B-00278bPure green teaTwinings200gMAY 201612 0000016009 UK 128China & AsiaSainsbury's 14B-00279Pure green teaTetley200g08 20153220Africa & AsiaMorrison's14B-00280Turkish sultanasCook with M & S500g03/2015L4079A520 3TurkeyMarks & Spencer14B-00281CurrantsCo-op500gNOV 2014L3295/11.13338GreeceCo-op14B-00282CurrantsSainsbury's500gFEB 2015L4128A7001GreeceSainsbury's 14B-00283Dried mixed fruitTesco500gMAR 20154055 N5 LOT: 21203UnknownTesco14B-00284Dried mixed fruitAsda 500gAPR 2015L4099N7371Produce of several countriesAsda14B-00285Chopped apricotsNatural Selection 200gJAN 20152A L4105/4 14120TurkeyAsda14B-00286Organic non-dairy rice drinkRice Dream Original Organic1 litre20.02.20150 052 M1European UnionHolland & Barrett14B-00287Rice drinkAlpro Rice Original1 litre09.02.15F2017European UnionTesco14B-00288Organic almond drinkEcoMil1 litre02/10/14PRO 02/04/1313092SpainHolland & Barrett14B-00289RaisinsMorrisons500gAPR 20154108 N5 LOT: 24293United StatesMorrison's14B-00290Organic sultanasWaitrose Organic375gOCT 2014L4112A 520 3TurkeyWaitrose 14B-00291Organic gluten free spaghettiDoves Farm Organic500g06/05/16Lot number 636 HItalySainsbury's 14B-00292Double choc browniesMrs Crimble'sPack of 409/09/2014L41470730534None declaredWaitrose 14B-00293CocoaCadbury's Bournville250g06.05.2016OCIO241931None declaredMorrison's14B-00294Crushed red chilliesRajah200g04 06 2016None declaredNone declaredMorrison's14B-00295Extra hot chilli powderEast End300gMAY 20164 133L1ANone declaredAsda14B-00296Chiili powder (extra hot)Indus 400gMAR 20164062-L3283None declaredTesco Extra14B-00297PaprikaEast End300gMAY 20164 136L1ANone declaredAsda14B-00298Paprika powderIndus 400gAPR 20164101-L4627None declaredTesco Extra14B-00299Ground gingerRajah85g24.04.2016None declaredNone declaredMorrison's14B-00300Hot whole round chilliesTRS150gMAY 2015CHW 13003IndiaSubru's Convenience Store14B-00301Chiili powderTRS400g25 JUNE 2015B030613IndiaSubru's Convenience Store14B-00302Ground gingerTRS400g31/03/2016P140311IndiaSubru's Convenience Store14B-00303Cinnamon powderTRS100g31-05-2016P140522IndiaSubru's Convenience Store14B-00304Paprika powderTRS400g14-04-16L-140409None declaredSubru's Convenience Store14B-00305Ceylon organic cinnamon powderSussex Wholefoods100gJul 201591233Sri Lankahealthysupplies.co.uk14B-00306Cinnamon powderFudco100gDec 2015Lot - 312181kChinaSathyam Supermarket14B-00307Dried chilliNiru500gAUG 2015120843None declaredSun Express14B-00308Crushed chilliesNatco300gAPR 2016140425-BN0045Prod: APR 2014IndiaKashmir Food Store14B-00309Crushed chilli flakes (hot)Fudco250g31 Mar 2015Lot - 413041kIndiaSun Express14B-00310Kashmiri (mild) chilli powderFudco250g31 Jan 2016Lot - 411051kIndiaSathyam Supermarket14B-00311aNutmeg powderFudco100gMar 2015Lot - 313080kNone declaredKashmir Food Store14B-00311bNutmeg powderFudco100gDec 2015Lot - 312132kNone declaredKashmir Food Store14B-00312Ginger powderFudco300gDec 2015Lot - 312131kNone declaredSathyam Supermarket14B-00313Ginger powderNatco400gAPR 2015130402-BN0006Prod: APR 2013ChinaKashmir Food Store14B-00314Red whole chillieSindhu500g05.03.2016JK/DE/0514/002Sri LankaSun Express14B-00315Organic cayenne pepperSteenbergs500gJun 201616157Indiastennbergs.co.uk14B-00316Cinnamonum zeylanicumJustIngredients500gJuly 201618179None declaredjustingredients.co.uk14B-00317Ground nutmegJustIngredients500gJuly 201612051Indonesiajustingredients.co.uk14B-00318Ground nutmegThe Vital Ingredient100gDEC 201413344 79734None declared14B-00319aCayenne pepperThe Vital Ingredient100gMAR 201514160 84094None declared14B-00319BbCayenne pepperThe Vital Ingredient100gSEP 201514157 84094None declared14B-00320CayenneCotswold Health Products1kgMarch 2016130024Indiarealfoods.co.uk14B-00321Nutmeg groundSuma500g01/1616556Indonesiarealfoods.co.uk14B-00322aPure green tea - 80 unbleached bagsClipper160g13/06/2016E1836Produce of several countriesSainsbury's 14B-00322bPure green tea - 80 unbleached bagsClipper160g13/07/2016M2160Produce of several countriesWaitrose14B-00322cPure green tea - 80 unbleached bagsClipper160g25/07/2016L2256Produce of several countriesSainsbury's Appendix 2, Table 1: Analytical results CategorySample NumberSample DescriptionBrandCitrinin (?g/kg)Sterigmatocystin (?g/kg)Fumonisin B1 (?g/kg)Fumonisin B2 (?g/kg)Fumonisin B3 (?g/kg)Ergometrine (?g/kg)Ergometrinine (?g/kg)Ergosine (?g/kg)Ergosinine (?g/kg)Ergocornine (?g/kg)Ergocorninine (?g/kg)Ergotamine (?g/kg)Ergotaminine (?g/kg)Ergocryptine (?g/kg)Ergocryptinine (?g/kg)Ergocristine (?g/kg)Ergocristinine (?g/kg)Alternariol (?g/kg)Tenuazonic Acid (?g/kg)AME (?g/kg)Altenuene (?g/kg)Altertoxin 1 (?g/kg)Tentoxin (?g/kg)Almond milk14B-00270Almond alternative to dairy milkTesco Free Fromnana<10<10<10nanananananananananananananananananaAlmond milk14B-00288Organic almond drinkEcoMilna<0.2<10<10<10<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Apple juice13B-02414Pressed apple juiceInnocent<0.2nananananananananananananananana<2<2<2<2<2<2Apple juice13B-02473Apple juice (made from concentrate)Centra<0.2nananananananananananananananana<2<2<2<2<2<2Apple juice13B-02496Pressed apple juiceDon Simon<0.2nananananananananananananananana<2<2<2<2<2<2Apple juice13B-02563Cloudy pressed apple juiceCawston Press<0.2nananananananananananananananana<2<2<2<2<2<2Apple juice13B-02565 English apple juice - Ida Red, mediumDuskin<0.2nananananananananananananananana<2<2<2<2<2<2Apple juice13B-02616Pressed apple juiceSuperValu<0.2nananananananananananananananana<2<2<2<2<2<2Apple juice13B-02619Sweet Worcester pressed apple juiceWatergull Orchards<0.2nananananananananananananananana<2<2<2<2<2<2Apple juice13B-02620Apple juice (from concentrate)Marks & Spencer<0.2nananananananananananananananana<2<2<2<2<2<2Apple juice13B-02621Pressed Bramley apple juiceSandringham Apple Juice<0.2nananananananananananananananana<2<2<2<2<2<2Apple juice14B-00189Cloudy apple juiceCopella<0.2nananananananananananananananana<2<2<2<2<2<2Apple juice14B-00244Biodynamic apple juiceOaklands Park Garden0.2nananananananananananananananana<2<2<2<2<2<2Asparagus13B-02424Green asparagus spearsKingfishernana<10<10<10nanananananananananananananananananaAsparagus13B-02449Asparagus bundleTesconana<10<10<10nanananananananananananananananananaAsparagus13B-02510Asparagus spearsAsdanana<10<10<10nanananananananananananananananananaAsparagus14B-00192Asparagus spearsSainsbury'snana<10<10<10nanananananananananananananananananaAsparagus14B-00193Bunched asparagusWaitrosenana<10<10<10nanananananananananananananananananaAsparagus14B-00251Asparagus Morrisonsnana<10<10<10nanananananananananananananananananaAsparagus14B-00269Bunched asparagusElveden Estatenana<10<10<10nanananananananananananananananananaBarley13B-02460Pearl barleyGreat Scot<0.2<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Barley13B-02508Pearl barleyWaitrose Love Life<0.2<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Barley13B-02530Pearl barleyMorrisons Wholefoods<0.2<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Barley13B-02571Pearl barleyCo-Op Wholefoods<0.2<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Barley13B-02586Pearl barleyCommunity Foods<0.2<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Barley13B-02632Mie?in?s kruopos (barley groats)S & S<0.2<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Barley14B-00177Pearl barleyJCR<0.2<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Barley14B-00206Pearl barleyMarks & Spencer<0.2<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Barley14B-00207Barley flakesNeal's Yard Wholefoods<0.2<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Barley14B-00228Dried barley (pudding)Jin Shin Foods<0.2<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Black olives13B-02427Pitted black Spanish olivesFragata<0.2nanananananananananananananananananananananaBlack olives13B-02428Pitted black olives in brineCrespo<0.2nanananananananananananananananananananananaBlack olives13B-02534Greek black olivesFOS<0.2nanananananananananananananananananananananaBlack olives13B-02575Black Gemlik olivesDurmaz<0.2nanananananananananananananananananananananaBlack olives13B-02576Dehydrated black olives - kuru seleMarmarabirlik<0.2nanananananananananananananananananananananaBlack olives13B-02584Kalamata olivesWaitrose<0.2nanananananananananananananananananananananaBlack olives13B-02601? La Grecque olivesTesco<0.2nanananananananananananananananananananananaBlack olives13B-02645Hojiblanca pitted black olivesHeliopolis<0.2nanananananananananananananananananananananaBlack olives14B-00178Pitted black olives in brineSiof<0.2nanananananananananananananananananananananaBlack olives14B-00187Sliced black olivesFigaro<0.2nanananananananananananananananananananananaBlack olives14B-00253Pitted black olivesKvuzat Yavne<0.2nanananananananananananananananananananananaBlack pepper13B-02406Ground black pepperSainsbury's<0.2<0.2nananananananananananananananananananananaBlack pepper13B-02407Whole black pepperMorrisons<0.2<0.2nananananananananananananananananananananaBlack pepper13B-02451Ground black pepperTesco Everyday Value<0.2<0.2nananananananananananananananananananananaBlack pepper13B-02579Ground black pepperKania Spices<0.2<0.2nananananananananananananananananananananaBlack pepper13B-02588Ground black pepperStonemill<0.2<0.2nananananananananananananananananananananaBlack pepper13B-02594Ground black pepperEast End<0.2<0.2nananananananananananananananananananananaBlack pepper13B-02623Whole black peppercorns (with grinder)Ko Spice<0.2<0.2nananananananananananananananananananananaBlack pepper14B-00174Poivre noir mouluMedia Food<0.2<0.2nananananananananananananananananananananaBlack pepper14B-00222Coarse black pepperRajah<0.2<0.2nananananananananananananananananananananaBlack pepper14B-00223Ground black pepperMillstone0.2<0.2nananananananananananananananananananananaBlack pepper14B-00226Black pepper groundSun Brand<0.2<0.2nananananananananananananananananananananaBlack Pepper14B-00175Black pepper powderTRS<0.2<0.2nananananananananananananananananananananaBlack tea14B-00273Loose teaPG Tipsnana<10<10<10nanananananananananananananananananaBlack tea14B-00274Assam tea bags - 100Tesco Finestnana<10<10<10nanananananananananananananananananaBlack tea14B-00275Earl Grey tea bagsTwiningsnana<10<10<10nanananananananananananananananananaBread13B-02422Stay fresh wholemeal sliced bread - mediumTescona<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2nanananananaBread13B-02468Plain breadSunblestna<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2nanananananaBread13B-02469Burger buns (6)Quickburyna<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2nanananananaBread13B-02544Wholemeal medium sliced breadHovisna<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2nanananananaBread13B-02569Sweet breadHeavenly Breadna<0.2nanana<2<23<2<2<23<2<2<22<2nanananananaBread13B-02577Large seeded loafGregg'sna<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2nanananananaBread13B-0260450/50 white bread with 50% wholemeal flourKingsmillna<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2nanananananaBread13B-02607Garlic + coriander naansCurrymatena<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2nanananananaBread14B-00201Mulit-seed & cereal pittasThe Food Doctorna<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2nanananananaBread14B-00202High bran sliced loafMarks & Spencerna<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2nanananananaBread14B-00232Wholemeal sliced breadBrace's Classicna<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2nanananananaBread14B-00245Medium sliced brown loafMorrison Saversna<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2nanananananaBread mix13B-02477Soda breadMortons Flourna<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2nanananananaBread mix13B-02506Oats 'n' bran bread flourWessex Millna<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2nanananananaBread mix13B-02507Wholemeal bread mixSainsbury'sna<0.2nanana<2<2<2<2<2<23<2<2<252nanananananaBread mix13B-02550Crusty wholemeal bread mixTescona<0.2nanana<2<2<2<2<2<2<2<2<2<23<2nanananananaBread mix13B-02589Crusty wholemeal bread mixThe Pantryna<0.2nanana<2<2<2<2<2<2<2<2<2<22<2nanananananaBread mix13B-02598Baker's Blend Sharpham Parkna<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2nanananananaBread mix13B-02610Mixed seed bread mixJames Martin Bakeryna<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2nanananananaBread mix14B-00236Malted brown bread mixCo-Opna<0.2nanana6<2<2<2<22<2<24<222nanananananaBread mix14B-00254White bread mixVictoria Foodsna<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2nanananananaBreakfast cereals13B-02420Frosted flakesCrownfield<0.2<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Breakfast cereals13B-02421Fruit loaded chunky granolaFuel<0.2<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Breakfast cereals13B-02474Irish muesliLifeforce<0.2<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Breakfast cereals13B-02475Toasted rice cerealSupervalu Rice Krunchies<0.2<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Breakfast cereals13B-02498Whole grain wheat cereal Nestlé Shredded Wheat<0.2<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Breakfast cereals13B-02523All bran originalKellogg's<0.2<0.2nanana<2<22<2<2<2<2<2<2223<2<2<2<2<2<2Breakfast cereals13B-02551Honey coated wholegrain wheat, corn and oat cerealTesco Multigrain Boulders<0.2<0.2nanana3<243<2333<2223<2<2<2<2<2<2Breakfast cereals13B-02580Multigrain hoopsGreat Start<0.2<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Breakfast cereals13B-02590Golden puffs (puffed wheat)Harvest Morn<0.2<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Breakfast cereals13B-02603Wheat branShire Foods<0.2<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Breakfast cereals13B-02655Organic whole wheat cerealWeetabix Organic<0.2<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Breakfast cereals14B-00213Fruit & fibreMarks & Spencer<0.2<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Buckwheat13B-02578Buckwheat flourDoves Farm <0.2<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Buckwheat13B-02633BuckwheatLimor0.4<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Buckwheat13B-02634Buckwheat flakesGalinta<0.2<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Buckwheat14B-00238Rolled buckwheat flakesWyedean Healthfoods<0.2<0.2nanana<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2Cardamom14B-00255Cardamom blackIndus <0.2<0.2nananananananananananananananananananananaCardomon14B-00176Green cardamomTRS<0.2<0.2nananananananananananananananananananananaCardomon14B-00224Dried cardamond seedsWah Loong Co. Ltd<0.2<0.2nananananananananananananananananananananaCardomon14B-00247Black cardamomsEast End<0.2<0.2nananananananananananananananananananananaCayenne pepper14B-00315Organic cayenne pepperSteenbergs<0.2<0.2nananananananananananananananananananananaCayenne pepper14B-00319aCayenne pepperThe Vital Ingredient<0.2<0.2nananananananananananananananananananananaCayenne pepper14B-00320CayenneCotswold Health Products<0.2<0.2nananananananananananananananananananananaCelon/Melange Tea14B-00181Cardamon teaAhmad Teanana<10<10<10nanananananananananananananananananaCherry juice13B-02415Apple & cherry pressed juiceMorrisons<0.2nanananananananananananananananananananananaCherry juice13B-02416Cherry juice drinkCherry Good<0.2nanananananananananananananananananananananaCherry juice13B-02417Cherries & berries juiceAsda<0.2nanananananananananananananananananananananaCherry juice13B-02485Cherry juice drinkAsda<0.2nanananananananananananananananananananananaCherry juice13B-02486Cherry juice 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chillieSindhu<0.2<0.2nananananananananananananananananananananaWine13B-02429Pinot grigio 2012 Delle VeneziePalastri Italianana<10<10<10nananananananananananana<2<2<2<2<2<2Wine13B-02430Garnacha rosé 2012Gran Familia Las Primasnana<10<10<10nananananananananananana<2<2<2<2<2<2Wine13B-02431California merlotOak Leafnana<10<10<10nananananananananananana<2<2<2<2<2<2Wine13B-02432Cherry wineCherry Bnana<10<10<10nananananananananananana<2<2<2<2<2<2Wine13B-02535Shiraz-Malbec 2011J. P. Chenetnana<10<10<10nananananananananananana<2<2<2<2<2<2Wine13B-02568Dornfelder light red wineBiddenden Gribble Bridgenana<10<10<10nananananananananananana<2<2<2<2<2<2Wine13B-02643Cabernet sauvignon 2011Wolf Blass Yellow Labelnana<10<10<10nananananananananananana<2<2<2<22<2Wine13B-02644Nettle wineLyme Bay Winerynana<10<10<10nananananananananananana<2<2<2<2<2<2Wine14B-00217Peach Garden Chardonnay 2012Marks & Spencernana<10<10<10nananananananananananana<2<2<2<2<2<2Wine14B-00218Shiraz & Mourvède 2013Fire Flowernana<10<10<10nananananananananananana<2<2<2<2<2<2Wine14B-00243Riesling 2012Devil's Rocknana<10<10<10nananananananananananana<2<2<2<2<2<2Appendix 3: Summary tables Table 1: Summary of Mycotoxin Occurrence in Products Analysed MycotoxinNumber (%) of samples in which mycotoxins were detectedCitrinin14/239 (6%)Alternaria toxins0/175 (0%)Fumonisins1/111 (1%)Sterigmatocystin6/200 (3%)Ergot Alkaloids15/122 (12%)Table 2: Summary of Mycotoxin Results MycotoxinTotal Number of samples analysedSamples in which mycotoxin was determined ≥ (LOQ)Range of results above LOQ(?g/kg)Citrinin 239140.2-0.8Alternaria toxins1750-Fumonisins111110Sterigmatocystin20060.2-0.7Ergot Alkaloids122152-21Appendix 4: Measurement Uncertainty, summary of recovery data and analytical methodology Table 1: Uncertainty of MeasurementMycotoxinUncertaintyFumonisins x ?g/kg ± 23%Sterigmatocystinx ?g/kg ± 19%Citrininx ?g/kg ± 20%Ergot Alkaloidsx ?g/kg ± 10%Alternaria toxinsx ?g/kg ± 8%Table 2: Summary of Recovery DataMycotoxinTotal Number of SamplesMean Recovery (%)RSD (%)Sterigmatocystin2398610Citrinin2009210Fumonisin B11111005Fumonisin FB21111013Fumonisin FB31111004Ergometrine 1221004Ergometrinine1221003Ergotamine1221002Ergotaminine1221012Ergosine1221013Ergosininine1221003Ergocristine1221002Ergocristinine1221012Ergocryptine1221012Ergocryptinine1221002Ergocornine1221003Ergocorninine1221002Alternariol1221004Tenuazonic Acid1751004AME1751004Altenuene1751004Altertoxin 11751004Tentoxin1751004Table 3: Analytical Methodology Applied ThroughoutMycotoxinClean-up ColumnDetermination MethodLimit of DetectionLimit of QuantificationUKAS AccreditedSterigmatocystinSPEHPLC (fluorescence)0.1?g/kg0.2?g/kgYesCitrininSPEHPLC (fluorescence)0.1?g/kg0.2?g/kgYesFumonisin B1, B2, B3.noneLC-MS/MS5?g/kg (each toxin)10?g/kg (each toxin)YesErgot Alkaloids (ergometrine, ergotamine, ergosine, ergocristine, ergocryptine and ergocornine and their (-inines))SPELC-MS/MS1?g/kg (each toxin)2?g/kg (each toxin)YesAlternaria toxins (alternariol,tenuazonic acid, AME, altenuene, altertoxin 1,tentoxin)SPELC-MS/MS1?g/kg (each toxin)2?g/kg (each toxin)YesRecovery criteria for all methods 70-110%.Appendix 5: Comments received from brandowners ................
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