Principles of Instrumental Analysis



Principles of Instrumental Analysis

5th Edition

Douglas A. Skoog - Stanford University

F. James Holler - University of Kentucky

Timothy A. Nieman - University of Illinois

Douglas A. Skoog and F. James Holler

Table of Contents

1. Introduction.

|Section I: Measurement Basics. |Web Resources |

|2. Electrical Components and Circuits. |Introduction |

|3. Operational Amplifiers in Chemical Instrumentation. |Treatment of data |

|4. Digital Electronics and Microcomputers. |Gravimetry |

|5. Signals and Noise. |Aqueous solutions |

|Section II: Atomic Spectroscopy. |Equilibrium calculations |

|6. An Introduction to Spectrometric Methods. |Titrimetry |

|7. Components of Optical Instruments. |Precipitate formation |

|8. An Introduction to Optical Atomic Spectrometry. |Complex-formation |

|9. Atomic Absorption and Atomic Fluorescence Spectrometry. |Acid/Base titrations |

|10. Atomic Emission Spectrometry. |Complex AB titrations |

|11. Atomic Mass Spectrometry. |Non-aqueous titrations |

|12. Atomic X-Ray Spectrometry. |Kinetic methods |

|Section III: Molecular Spectroscopy. |Electrochemistry |

|13. An Introduction to Ultraviolet/Visible Molecular Absorption |REDOX titrations |

|Spectrometry. |Potentiometry |

|14. Applications of Ultraviolet/Visible Molecular Absorption |Coulometry |

|Spectrometry. |Voltammetry |

|15. Molecular Luminescence Spectrometry. |Spectrophotometry |

|16. An Introduction to Infrared Spectrometry. |Molecular spectroscopy |

|17. Applications of Infrared Spectrometry. |Spectroscopy equipment |

|18. Raman Spectroscopy. |Atomic spectroscopy |

|19. Nuclear Magnetic Resonance Spectroscopy. |Mass Spectroscopy |

|20. Molecular Mass Spectrometry. |Solvent extraction |

|21. Surface Characterization by Spectroscopy and Microscopy. |Chromatography |

|Section IV: Electroanalytical Chemistry. |Gas chromatography |

|22. Introduction to Electroanalytical Chemistry. |Liquid chromatography |

|23. Potentiometry. |Hyphenated methods |

|24. Coulometry. | |

|25. Voltammetry. | |

|Section V: Separation Methods. | |

|26. An Introduction to Chromatographic Separations. | |

|27. Gas Chromatography. | |

|28. High-Performance Liquid Chromatography. | |

|29. Supercritical Fluid Chromatography and Extraction. | |

|30. Capillary Electrophoresis and Capillary Electrochromatography. | |

|Section VI: Miscellaneous Methods. | |

|31. Thermal Methods. | |

|32. Radiochemical Methods. | |

|33. Automated Methods of Analysis. | |

|Appendix A: Evaluation of Analytical Data. | |

|Appendix B: Activity Coefficients. | |

|Appendix C: Some Standard and Formal Electrode Potentials. | |

|Appendix D: Compounds for Preparing Standard Solutions of Some Common | |

|Elements. | |

|Appendix E: Common Acronyms Encountered in Chemical Instrumentation. | |

|Appendix F: Answers to Selected Problems Index. | |

Introduction

X-rays

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