Chemical Engineering
DEENBANDHU CHHOTU RAM UNIVERSITY OF SCIENCE & TECHNOLOGY,
MURTHAL (SONEPAT)
SCHEME OF STUDIES & EXAMINATIONS
B.Tech. 3rd YEAR (SEMESTER – V) (CHEMICAL ENGINEERING)
Choice Based Credit Scheme w.e.f. 2020-21
|S. No. | |Course Title |Teaching Schedule |Marks of |Examination Marks |Total |Credit |Duration of |
| |Course No. | | |Class work | | | |Exam |
| | | |L |T |P | |Theory |Practical| |
CORE ELECTIVE-II:
1. CHE350C: NANOSCIENCE FOR CHEMICAL ENGINEERS
2. CHE352C: RENEWABLE ENERGY
3. CHE354C: POLYMER SCIENCE & ENGINEERING
4. CHE356C: ADVANCED SEPARATION PROCESSES
OPEN ELECTIVE-I:
1. HUM SOFT SKILLS AND INTER PERSONAL COMMUNICATION
2. HUM201C PROFESSIONAL COMMUNICATION FOR ENGINEERS
3. MGT HUMAN RESOURCE MANAGEMENT
4. HUM INTRODUCTION TO LANGUAGE (GERMAN)
5. HUM INTRODUCTION TO LANGUAGE (FRENCH)
Note:
1. The students will be allowed to use non-programmable scientific calculator. However, sharing/exchange of calculator is prohibited in the examination.
2. Electronics gadgets including Cellular phones are not allowed in the examination.
3. Each student has to undergo Professional training of 4-6weeksfrom the industry, institute, research lab, training center etc during summer vacation and its evaluation shall be carried out in the VII semester.
4. Students will be permitted to opt for any one core elective run by the department.
5. Students will be permitted to opt for any one open elective run by the other department. However, the departments will offer those elective for which they have expertise. The choice of the students for any elective shall not be a binding for the department to offer, if the department does not have expertise. The minimum strength of the students should be 20 to run an elective course.
|B. Tech. Semester – V (Chemical Engineering) |
|CHE301C : CHEMICAL REACTION ENGINEERING-I |
|L |T |P |Credits | |Class Work |: |25 Marks |
|3 |1 |- |4 | |Examination |: |75 Marks |
| | | | | |Total |: |100 Marks |
| | | | | |Duration of Examination |: |3 Hours |
Course Objectives: To learn:
• Basic concepts of kinetics and rate laws.
• Design and rating of ideal reactors including heat effects.
• Interpretation of rate data.
• Design and rating of reactors involving multiple reactions including heat effects.
• Analysis of non-ideal flow behaviour in reactors.
Course Outcomes: Students will be able to:
• Design chemical reactors involving heat effects optimally using minimum amount of data.
• Fix some problems related to operability and productivity.
• Operate reactors in a safe manner for single and multiple reactions.
• Analyze the non-ideality in the reactors.
Syllabus contents:
UNIT-I: Kinetics of homogeneous reaction: concepts of rate equation, order and molecularity, Elementary and Non-elementary Reactions, Kinetic Models for Non-elementary Reactions. Interpretation of Batch Reactor Data, Constant and Variable volume Batch Reactor; Introduction to reactor design.
UNIT-II: Ideal Reactors: Batch, CSTR and PFR, Design or performance equation for Ideal Reactors; Design for Single Reactions: Size Comparison of Single Reactors, Multiple-Reactor Systems, Recycle Reactor, Autocatalytic Reactions.
UNIT-III: Design for Multiple Reaction: Parallel and Series reactions, Qualitative and Quantitative discussion about product Distribution. Temperature and Pressure Effects in single reactions: General Graphical Design Procedure, Optimum Temperature Progression, Adiabatic and Nonadiabatic operations, Exothermic reaction in Mixed Flow Reactors; Multiple reactions.
UNIT-IV: Non-Ideal Flow: RTD, experimental methods for determination of RTD, Dispersion Model, Tanks-in- Series Model..
TEXT BOOKS:
1. Elements of Chemical Reaction Engineering by H. Scott Fogler, 2nd Edition, Prentice Hall 2001.
2. Chemical Reaction Engineering by Octave Levenspiel, 3rd Edition, John Wiley & Sons 2001.
REFERENCE BOOKS:
1. Kinetics and Mechanisms of Chemical Transformation: J. Rajaram and J. C. Kuriacose-Macmillan India Ltd. New Delhi.
2. Chemical Engineering Kinetics: J.M. Smith-Mcgraw-Hill Book Company, New Delhi. J. Geankoplis, Transport Processes and Unit Operations, 3rd Edition, Prentice Hall, India, 1993.
NOTE:
1. Part A: Till academic session 2020-2021:
In the semester examination, the examiner will set 08 questions in all selecting two from each unit. The candidates will be required to attempt five questions in all selecting at least one from each unit. All questions will carry equal marks.
Part B: From Academic Session 2021-2022 onwards: For the semester examination, nine questions are to be set by the examiner. Question no. 1, containing 6-7 short answer type questions, will be compulsory & based on the entire syllabus. Rests of the eight questions are to be set by setting two questions from each of the four units of the syllabus. The candidates will be required to attempt five questions in all, selecting one from each unit. All questions will carry equal marks.
2. The students will be allowed to use non-programmable scientific calculator. However, sharing/exchange of calculator is prohibited in the examination.
3. Electronics gadgets including Cellular phones are not allowed in the examination.
|B. Tech. Semester – V (Chemical Engineering) |
|CHE303C : TRANSPORT PHENOMENA |
|L |T |P |Credits | |Class Work |: |25 Marks |
|3 |1 |- |4 | |Examination |: |75 Marks |
| | | | | |Total |: |100 Marks |
| | | | | |Duration of Examination |: |3 Hours |
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Course Objectives: This course will highlight coupling between three transport phenomena with applications in various disciplines in engineering and science, and will demonstrate to the students the common mathematical structure of transport problems. The course will deal with flow problems involving Newtonian and non-Newtonian fluids, solid-state heat conduction, forced and free convection, binary diffusion with or without chemical reaction.
Course Outcomes: Students would be familiar with:
• Basics of vector and tensor analysis.
• Be able to solve transport problems using shell balances.
• Formulate and solve one-dimensional transport problems by using the conservation equations.
• Formulate simple multi-dimensional transport problems.
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Syllabus contents:
UNIT-I : Introduction to Transport Phenomena: Vector and Tensor Analysis: Basic concepts, Formulation of transport problems from nature, Basics of momentum transport, Euler/Lagrangian viewpoint, laminar and turbulent flows, Boundary layers, stress tensor, dimensional analysis, Shell momentum balances, equations of change, applications to isothermal flow of Newtonian & non-Newtonian fluids.
UNIT-II: Basics of energy transport: conductive, convective and viscous dissipation energy fluxes.
Equations of change for non-isothermal systems and applications to steady-state conduction and convection, Heat sources, fins, Free and forced convection.
UNIT-III: Basics of mass transport: mechanisms, and mass and molar fluxes.
Derivation of equation of continuity for a binary mixture and its application to convection-diffusion problems, Shell balance approach for mass transfer problems, Problems of diffusion with chemical reaction in porous catalyst.
UNIT-IV : Unsteady-state: momentum, heat and mass transport, formulation of basic equations and similarity transform method, Applications like flow near a wall suddenly set in motion, heating of semi- infinite slab, heating of a finite slab, unsteady diffusion.
TEXT BOOKS:
1. R. B. Bird, W. E. Stewart, and E. S. Lightfoot. Transport Phenomena, 2nd ed., Wiley India Pvt. Ltd.
2. Welty, C. E. Wicks, R. E. Wilson, and G. L. Rorrer. Fundamentals of Momentum, Heat, and Mass Transfer. 5th ed., Wiley India Pvt. Ltd.
REFERENCES BOOKS:
1. W. M. Deen, Analysis of Transport Phenomena, Oxford University Press.
2. W. J. Thompson, Introduction to Transport Phenomena, Prentice Hall.
NOTE:
1. Part A: Till academic session 2020-2021:
In the semester examination, the examiner will set 08 questions in all selecting two from each unit. The candidates will be required to attempt five questions in all selecting at least one from each unit. All questions will carry equal marks.
Part B: From Academic Session 2021-2022 onwards: For the semester examination, nine questions are to be set by the examiner. Question no. 1, containing 6-7 short answer type questions, will be compulsory & based on the entire syllabus. Rests of the eight questions are to be set by setting two questions from each of the four units of the syllabus. The candidates will be required to attempt five questions in all, selecting one from each unit. All questions will carry equal marks.
2. The students will be allowed to use non-programmable scientific calculator. However, sharing/exchange of calculator is prohibited in the examination.
3. Electronics gadgets including Cellular phones are not allowed in the examination.
|B. Tech. Semester – V (Chemical Engineering) |
|CHE305C : MASS TRANSFER-I |
|L |T |P |Credits | |Class Work |: |25 Marks |
|3 |1 |- |4 | |Examination |: |75 Marks |
| | | | | |Total |: |100 Marks |
| | | | | |Duration of Examination |: |3 Hours |
Course Objectives: Basic concepts of Mass Transfer, Staged and Continuous Contact equipment design, gas absorption, humidification and drying.
Course Outcomes: Students will be:
• Able to design staged and continuous contactors.
• Familiar with cooling towers, drying, absorption, humidification.
Syllabus contents:
UNIT-I: Diffusion in gases and liquids, Equation of continuity. Theories of mass transfer, Individual and overall mass transfer coefficients, Mass, heat and momentum transfer analogies. Simultaneous heat and mass transfer.
UNIT-II: Mass balance in co-current and counter-current continuous contact equipments. Continuous contact equipments. Gas absorption: Principles of Absorption, Tower packings, Limiting flow rates; Loading and Flooding. Stage efficiencies. HTU and NTU concepts. Design of Absorption Tower.
UNIT-III: Humidification: Humidity, Wet-Bulb temperature, Lewis relation Dew point, Adiabatic saturation temperature, Humidity chart, Cooling Towers. Theory and calculation of Humidification Processes.
UNIT-IV: Drying: Principles of Drying, Rate of drying curves, Time of Drying, Batch Drying, Cross- circulation drying, Through- circulation drying, Continuous drying, Drying Equipment.
TEXT BOOKS:
1. Binay K.Dutta, Principles of Mass Transfer and Separation Processes, 2nd edition, Prentice Hall of India, 2007.
2. R.E.Treybal, Mass Transfer Operations, 3rd Edition, Mc-Graw Hill, New Delhi, 1983.
3. E.D. Cussler, Diffusion - Mass Transfer in Fluid Systems, Cambridge University Press, Cambridge 1984.
REFERENCE BOOKS:
1. C.J. Geankoplis, Transport Processes and Unit Operations, 3rdEdition, Prentice Hall, India, 1993.
2. S. Foust, Principles of Unit Operations, 2nd Edition, Wiley, New York, 1980.
NOTE:
1. Part A: Till academic session 2020-2021:
In the semester examination, the examiner will set 08 questions in all selecting two from each unit. The candidates will be required to attempt five questions in all selecting at least one from each unit. All questions will carry equal marks.
Part B: From Academic Session 2021-2022 onwards: For the semester examination, nine questions are to be set by the examiner. Question no. 1, containing 6-7 short answer type questions, will be compulsory & based on the entire syllabus. Rests of the eight questions are to be set by setting two questions from each of the four units of the syllabus. The candidates will be required to attempt five questions in all, selecting one from each unit. All questions will carry equal marks.
2. The students will be allowed to use non-programmable scientific calculator. However, sharing/exchange of calculator is prohibited in the examination.
3. Electronics gadgets including Cellular phones are not allowed in the examination.
|B. Tech. Semester – V (Chemical Engineering) |
|CHE307C : PROCESS INSTRUMENTATION |
|L |T |P |Credits | |Class Work |: |25 Marks |
|3 |- |- |3 | |Examination |: |75 Marks |
| | | | | |Total |: |100 Marks |
| | | | | |Duration of Examination |: |3 Hours |
Course Objectives: To learn about:
• Basic elements of an instrument along with its static and dynamic characteristics.
• Various types of industrial thermometers.
• Basic concepts of various types of composition analysis.
• Various types of instruments for measurement of pressure, vacuum, head, density, level and flow measurement.
• An overview of various recording, indicating and signaling instruments, transmission of instrument readings, instrumentation diagrams, control center.
Course Outcomes: Students will be able to:
• To understand the basic principles of various instruments used in industry.
• To analyze the need of different process instruments for various processes.
Syllabus contents:
UNIT-I: General principles of measurement: Static and Dynamic characteristics of instruments, sensors & transducers.
Process instruments: Recording instruments, indicator and signaling instruments transmission of instrument reading, control centre, instrumentation diagram, online instrumentation in modern plants.
UNIT-II: Temperature measurement: Thermocouples, resistance thermometers, bimetallic thermometers, thermistors, optical and radiation pyrometer.
Pressure measurement: Use of manometer, Bourdon gauge, Bellows type gauge, measurement of vacuum, pressure transducers.
UNIT-III: Flow measurement: Use of obstruction type meters, variable area meters, pressure probes, positive displacement type meters, electromagnetic flowmeters and mass flow meters.
Liquid level measurement: Direct and differential method for the measurement in open pressure vessels.
UNIT-IV: Instrument for gas analysis: gas chromatography, mass spectroscopy.
Miscellaneous measurements: Composition measurement, measurement of viscosity, conductivity, humidity, pH and nuclear radiations.
TEXT BOOKS:
1. Industrial Instrumentation: D.P. Eckmen - John Wiley.
2. Instrumentation in Process Control: W.J. Wightmen - Butterworth.
REFERENCE BOOKS:
1. Applied Instrumentation in the Process Industries Vol-I & II: W.G. Andrew - Gulf Publishing Company.
2. Process Instrumentation and Control Hand Book : J.M. Douglas - McGraw Hill.
3. Hand Book of Measurement Science: P.H. Sydenaam - John Wiley.
NOTE:
1. Part A: Till academic session 2020-2021:
In the semester examination, the examiner will set 08 questions in all selecting two from each unit. The candidates will be required to attempt five questions in all selecting at least one from each unit. All questions will carry equal marks.
Part B: From Academic Session 2021-2022 onwards: For the semester examination, nine questions are to be set by the examiner. Question no. 1, containing 6-7 short answer type questions, will be compulsory & based on the entire syllabus. Rests of the eight questions are to be set by setting two questions from each of the four units of the syllabus. The candidates will be required to attempt five questions in all, selecting one from each unit. All questions will carry equal marks.
2. The students will be allowed to use non-programmable scientific calculator. However, sharing/exchange of calculator is prohibited in the examination.
3. Electronics gadgets including Cellular phones are not allowed in the examination.
|B. Tech. Semester – V (Chemical Engineering) |
|CHE309C : PROCESS UTILITIES & SAFETY |
|L |T |P |Credits | |Class Work |: |25 Marks |
|3 |- |- |3 | |Examination |: |75 Marks |
| | | | | |Total |: |100 Marks |
| | | | | |Duration of Examination |: |3 Hours |
Course Objectives: Basic concepts of Process utilities, Heat transfer media, steam traps, compressors. Industrial hazards and HAZOP etc.
Course Outcomes: Students will be:
• Able to understand process utilities, Industrial hazards, Disaster Management and HAZOP.
• Familiar with Heat transfer media, Refrigerators and Refrigeration System, piping networks for water, steam condensate and air Utilisation, Hazards, Disaster management.
Syllabus contents:
UNIT-I: Heat Transfer Media-Characteristic properties, classification, selection & their industrial applications. Utilities, Refrigeration, Steam System - Applications, design of efficient steam heating systems, condensate utilization and flash steam, steam Traps.
UNIT-II: Air, Reciprocating air compressors, vacuum pumps, air receivers, different types of ejectors and barometric condensers, piping networks for water, steam condensate and air Utilization. Water, its characteristics and conditioning for process industries, e.g. boiler feed, cooling etc. Recycling aspects of water.
UNIT-III: Hazards - Introduction, hazards due to fire explosion, toxicity and radiation, chemical hazards, maximum allowable concentration and threshold limiting values, protective and preventive measures in hazard control.
UNIT-IV: Disaster management - Scale of disaster, vapour cloud explosion, relief system emergency plans, standard safety programmes for disaster control, HAZOP analysis of plants. Indian legislation for safety and hazards, safety codes.
TEXT BOOKS:
1. Chemical Process Safety Fundamentals with Applications: D.A. Crowl and J.F. Louvar - Prentice Hall.
REFERENCE BOOKS:
1. Loss Prevention in process Industry: F.P. Lees Vol I, II, III - Butterworths.
2. Safety in Process Design: G.C. Wells - John Wiley.
3. Refrigeration & Air conditioning: Manohar Prasad, New Age International Publishers.
4. Heat Transfer principles & Applications: B K Dutta, PHI.
NOTE:
1. Part A: Till academic session 2020-2021:
In the semester examination, the examiner will set 08 questions in all selecting two from each unit. The candidates will be required to attempt five questions in all selecting at least one from each unit. All questions will carry equal marks.
Part B: From Academic Session 2021-2022 onwards: For the semester examination, nine questions are to be set by the examiner. Question no. 1, containing 6-7 short answer type questions, will be compulsory & based on the entire syllabus. Rests of the eight questions are to be set by setting two questions from each of the four units of the syllabus. The candidates will be required to attempt five questions in all, selecting one from each unit. All questions will carry equal marks.
2. The students will be allowed to use non-programmable scientific calculator. However, sharing/exchange of calculator is prohibited in the examination.
3. Electronics gadgets including Cellular phones are not allowed in the examination.
B. Tech. Semester – V (Chemical Engineering)
CHE351C : CHEMICAL TECHNOLOGY
|L |T |P |Credits | |Class Work |: |25 Marks |
|3 |- |- |3 | |Examination |: |75 Marks |
| | | | | |Total |: |100 Marks |
| | | | | |Duration of Examination |: |3 Hours |
Course Objectives: The main objective is to
• Give comprehensive study of the different chemical industries involving process technology, availability of raw materials, production trends, preparation of flow sheet, engineering problems involving ,material of construction, environmental pollution, waste utilization, economic aspects etc.
• To familiarize the students with the basic concepts involved in manufacturing process of various industrial gasses, sulphur, nitrogen industries, fertilizers, glass, cement, paint, paper & pulp, sugar etc.
• To show students a comprehensive picture of chemical industries.
Course Outcomes: Students will be able to
• State basic principles of chemical process industry
• Understand various processes used for manufacturing different compounds
• Draw different types of flow sheets used in process industries
• Describe engineering problems of various chemical industries.
• Understand various equipments/instruments used in process industries
Syllabus contents:
UNIT-I: Introduction of chemical process industries with reference to Indian resources, Process symbols used for various equipments. Industrial gases: Oxygen, hydrogen, producer gas, nitrogen and carbon dioxide. Sulphur industries: Sulphuric acid and oleum.
UNIT-II: Nitrogen industries: Ammonia, nitric acid, nitrogenous and mixed fertilizers. Chlor-Alkali industries: caustic soda, chlorine, hydrochloric acid, soda ash. Phosphorous industries: Phosphorous, phosphoric acid, super- phosphates.
UNIT-III: Ceramic industries: Portland cement, glass. Sugar Industry. Fermentation Industries: Alcohol, beer, wine, citric acid, lactic acid. Surface-coating Industries: Paints, pigments.
UNIT-VI: Pulp and paper: Different Pulping processes, recovery of chemicals, stock preparation and paper making. Soap & detergents, glycerin. Agrochemical Industries: Insecticides, herbicides, Pesticides,
TEXT BOOKS:
1. Outlines of Chemical Technology, C.E. Dryden - East - West Press Pvt. Ltd., New
Delhi.
2. Shreve's Chemical Process Industries , G.T. Austin McGraw- Hill Book Company, New
Delhi.
REFERENCE BOOKS:
1. A text Book of Chemical Technology, S.D. Shukla and G.N. Pandey - Vol.-II Vikas
Publishing House Pvt.Ltd., New Delhi.
2. Industrial Chemical, W.L. Faith, D.B. Keyes and R.L. Clark - John Wiley.
3. Chemical process industries, W.V.Mark, edited By S.C.Bhatia, vol. 2, 2nd ed:, CBS publisher & distributor, New Delhi. N
NOTE:
1. Part A: Till academic session 2020-2021:
In the semester examination, the examiner will set 08 questions in all selecting two from each unit. The candidates will be required to attempt five questions in all selecting at least one from each unit. All questions will carry equal marks.
Part B: From Academic Session 2021-2022 onwards: For the semester examination, nine questions are to be set by the examiner. Question no. 1, containing 6-7 short answer type questions, will be compulsory & based on the entire syllabus. Rests of the eight questions are to be set by setting two questions from each of the four units of the syllabus. The candidates will be required to attempt five questions in all, selecting one from each unit. All questions will carry equal marks.
2. The students will be allowed to use non-programmable scientific calculator. However, sharing/exchange of calculator is prohibited in the examination.
3. Electronics gadgets including Cellular phones are not allowed in the examination.
|B. Tech. Semester – VII (Chemical Engineering) |
|CHE353C : SUSTAINABILITY ENGINEERING |
|L |T |P |Credits | |Class Work |: |25 Marks |
|3 |- |- |3 | |Examination |: |75 Marks |
| | | | | |Total |: |100 Marks |
| | | | | |Duration of Examination |: |3 Hours |
Course Objectives:
• To understand the role of engineering and technology within sustainable development.
• To know the methods, tools, and incentives for sustainable product service system development.
• To establish a clear understanding of the role and impact of various aspects of engineering decisions on environmental societal and economic problems.
Course Outcomes:
• Able to understand the different types of environmental pollution problems and their sustainable solutions.
• Able to work in the area of sustainability for research and education.
• Having a broader perspective in thinking for sustainable practices by utilizing the engineering knowledge and principles gained from this course.
Syllabus contents:
UNIT-I: Introduction (types of pollution, water standards for potable and agricultural streams, air standards, Environmental disturbances, public awareness and action, population and economic growth, Industrialization, Energy growth, Manmade disturbances Introduction to the idea of sustainability and its relevance, status of environment-environmental, Social and economical issues, need for sustainability, ways to achieve sustainability-population, resources, development and environment, concept of sustainability factors governing sustainable development, determinants of sustainable development, local and global challenges for sustainable development, clean development mechanism (CDM), Environmental legislations in India-water, air act, solid waste management.
UNIT-II: Air and water pollution, sources and effects, sustainable treatment methods, solid waste-sources, effects of solid waste, leachate, hazardous waste, e-waste, plastic waste, zero waste concept, 3 R concept, Global environmental issues-Resources degradation, climate change, global warming, ozone layer depletion, carbon credits, carbon trading, carbon footprints.
UNIT-III: Tools used to ensure sustainability in engineering activities- environmental management systems, environmental management standards, ISO 14000 series, Life cycle analysis (LCA), and environmental impact assessment- Procedure of EIA in India. Basic concept of sustainable habitat, green buildings, green material for building construction, materials selection for sustainable design, methods for increasing energy efficiency of buildings, sustainable cities, sustainable transport.
UNIT-IV: Sustainable sources of energy: basic concept conventional and non-conventional, sources, solar, fuel cells, wind energy, small hydro plants, bio fuels, energy derived from oceans, geothermal energy, energy conservation, green engineering, sustainable urbanization.
TEXT BOOKS:
1. Sustainable Engineering: Drivers, Metrics, Tools, and Applications 1st Edition by Krishna R. Reddy (Author), Claudio Cameselle (Author), Jeffrey A. Adams (Author), Publisher: Wiley; 1 edition (April 30, 2019), ISBN-13: 978-1119493938.
2. Sustainability Engineering: A Design Guide for the Chemical Process Industry, Authors: Perl, Jeffery, Springer International Publishing, 978-3-319-32493-7, Edition Number 01.
REFERENCE BOOKS:
1. Sustainability Engineering: concepts, Design and Case studies, by Allen, D.T. and Shonnard, D. R, Prentice Hall, 1 edition (December 30, 2011).
2. Basic concepts in Environmental Management by Mackenthun, K. M, , Lewis Publication, London, 1998.
3. Environmental Impact Assessment Guidelines , latest Notification of Government of India.
4. ECBC code, Bureau of Energy Efficiency, New Delhi Bureau of Energy Efficiency publications-Rating system, TERI publication, GRIHA Rating system.
NOTE:
1. In the semester examinations, examiner is required to set up question paper covering the entire syllabus in accordance with the examination reforms circulated by the AICTE & approved under item No. 14_18 of academic council.
2. In the semester examination, the examiner will set 08 questions in all selecting two from each unit. The candidates will be required to attempt five questions in all selecting at least one from each unit. All questions will carry equal marks.
3. The students will be allowed to use non-programmable scientific calculator. However, sharing/exchange of calculator is prohibited in the examination.
4. Electronics gadgets including Cellular phones are not allowed in the examination.
|B. Tech. Semester – V (Chemical Engineering) |
|CHE355C : ENERGY TECHNOLOGY |
|L |T |P |Credits | |Class Work |: |25 Marks |
|3 |- |- |3 | |Examination |: |75 Marks |
| | | | | |Total |: |100 Marks |
| | | | | |Duration of Examination |: |3 Hours |
Course Objectives: Basic concepts of Solid Fuels, Liquid Fuels, Gaseous Fuels Classification of coals, Alternate Energy System like Solar Energy, bio fuels, biodiesel, Biogas etc.
Course Outcomes: Students will be
• Able to understand Solid Fuels, Liquid Fuels, Gaseous Fuels.
• Familiar with coal carbonization, cracking, reforming, L.P.G., Water Gas, Producer Gas, fuel cells, hydrogen energy etc.
Syllabus contents:
UNIT-I: Solid Fuels: Classification of coals, origin, composition, characteristics of coal, washing, storage of coal, pulverized fuel, coal carbonization, properties of coal.
UNIT-II: Liquid Fuels: Origin, composition, classification of petroleum, processing of crude oil, cracking, reforming, octane & cetane number, purification of petroleum products, properties of petroleum products.
UNIT-III: Gaseous Fuels: Natural gas, L.P.G., Water Gas, Producer Gas, Flue Gas analysis. Combustion: General principles of combustion, types of combustion processes, Burners, combustion calculation.
UNIT-IV: Alternate Energy System: Solar Energy and its applications, wind energy, geothermal energy, fuel cells, tidal energy, wave energy, hydrogen energy, Biomass, bio fuels, biodiesel, Biogas, biogas plants, biomass gasification.
TEXT BOOKS:
1. Elements of Fuels, Furnaces and Refractories: O.P. Gupta- Khanna Publishers
2. Energy Technology: S.Rao, B.B. Parulekar- Khanna Publisher.
REFERENCE BOOKS:
1. Fuels & Combustion: S. Sarkar - Longman Publishers India Ltd. - IInd Edition.
2. Fuels and their combustion: R.T. Haslam and R.P. Russel- McGraw-Hill.
3. Renewable Energy Resources: J. Twindell and Tonyweir- E & F Nspon.
NOTE:
1. Part A: Till academic session 2020-2021:
In the semester examination, the examiner will set 08 questions in all selecting two from each unit. The candidates will be required to attempt five questions in all selecting at least one from each unit. All questions will carry equal marks.
Part B: From Academic Session 2021-2022 onwards: For the semester examination, nine questions are to be set by the examiner. Question no. 1, containing 6-7 short answer type questions, will be compulsory & based on the entire syllabus. Rests of the eight questions are to be set by setting two questions from each of the four units of the syllabus. The candidates will be required to attempt five questions in all, selecting one from each unit. All questions will carry equal marks.
2. The students will be allowed to use non-programmable scientific calculator. However, sharing/exchange of calculator is prohibited in the examination.
3. Electronics gadgets including Cellular phones are not allowed in the examination.
|B. Tech. Semester – V (Chemical Engineering) |
|CHE357C : COMPUTATIONAL FLUID DYNAMICS |
|L |T |P |Credits | |Class Work |: |25 Marks |
|3 |- |- |3 | |Examination |: |75 Marks |
| | | | | |Total |: |100 Marks |
| | | | | |Duration of Examination |: |3 Hours |
Course Objectives: Basic concepts of Solid Fuels, Liquid Fuels, Gaseous Fuels Classification of coals, Alternate Energy System like Solar Energy, bio fuels, biodiesel, Biogas etc.
Course Outcomes: Students will be
• Able to understand Solid Fuels, Liquid Fuels, Gaseous Fuels.
• Familiar with coal carbonization, cracking, reforming, L.P.G., Water Gas, Producer Gas, fuel cells, hydrogen energy etc.
Syllabus contents:
UNIT-I: Introduction to Computational Fluid Dynamics and Principles of Conservation: Continuity Equation, Navier Stokes Equation, Energy Equation and General Structure of Conservation Equations and boundary conditions. Classification of Partial Differential Equations and Physical Behavior, Approximate Solutions of Differential Equations: Error Minimization Principles, Variational Principles and Weighted Residual Approach, Fundamentals of Discretization: Finite Element Method, Finite Difference and Finite Volume Method.
UNIT-II: Finite Volume Method: Some Conceptual Basics and Illustrations through 1-D Steady State Diffusion Problems, Boundary Condition Implementation . Discretization of Unsteady State Problems, Important Consequences of Discretization of Time Dependent Diffusion Type Problems and Stability Analysis : Consistency, Stability and Convergence, , Grid independent and time independent study Solution methods for multiphase flow, Stability analysis of parabolic equations, one dimension unsteady state diffusion problems.
UNIT-III: Stability analysis of hyperbolic equations, Finite Volume Discretization of 2-D unsteady State Diffusion
type Problems, Solution of Systems of Linear Algebraic Equations: Elimination Methods, Iterative Methods, Gradient Search Methods, Discretization of Convection-Diffusion Equations: A Finite Volume Approach, Discretization of Navier Stokes Equations, SIMPLE Algorithm, SIMPLER Algorithm.
UNIT-IV: Introduction to Turbulence Modeling, Important features of turbulent flow, Vorticity transport equation, Statistical representation of turbulent flows: Homogeneous turbulence and isotropic turbulence, General Properties of turbulent quantities, Reynolds average Navier stokes (RANS) equation, Closure problem in turbulence: Necessity of turbulence modeling, Different types of turbulence model, Eddy viscosity models, Mixing length model, Turbulent kinetic energy and dissipation, The κ-ε model, Advantages and disadvantages of κ -ε model, More two-equation models: RNG κ-ε model and κ-ω model, Reynolds stress model (RSM),Large eddy Simulation (LES),DNS (Direct numerical simulation)
TEXT BOOKS:
1. S.V. Patankar, Numerical Heat Transfer and Fluid Flow, McGraw-Hill.
2. H.K.Versteeg & W. Malalasekera, An Introduction to Computational Fluid Dynamics, Longman Scientific & Technical.
3. John C. Tannehill, Dale A. Anderson and Richard H. Pletcher, Computational Fluid Mechanics and Heat Transfer, Taylor &Francis.
4. Jiyuan Tu Guan Heng Yeoh Chaoqun Liu ,Computational Fluid Dynamics, 3rd Edition, A Practical Approach Authors: Paperback ISBN: 9780081011270 eBook ISBN: 9780081012444 Imprint: Butterworth-Heinemann Published Date: 26th January 2018
REFERENCE BOOKS:
1. J. H. Ferziger and M.Peric, Computational Methods for Fluid Dynamics, Springer.
2. John D.Anderson Jr, Computational Fluid Dynamics, McGraw Hill Book Company.
NOTE:
4. Part A: Till academic session 2020-2021:
In the semester examination, the examiner will set 08 questions in all selecting two from each unit. The candidates will be required to attempt five questions in all selecting at least one from each unit. All questions will carry equal marks.
Part B: From Academic Session 2021-2022 onwards: For the semester examination, nine questions are to be set by the examiner. Question no. 1, containing 6-7 short answer type questions, will be compulsory & based on the entire syllabus. Rests of the eight questions are to be set by setting two questions from each of the four units of the syllabus. The candidates will be required to attempt five questions in all, selecting one from each unit. All questions will carry equal marks.
5. The students will be allowed to use non-programmable scientific calculator. However, sharing/exchange of calculator is prohibited in the examination.
6. Electronics gadgets including Cellular phones are not allowed in the examination.
|B. Tech. Semester – V (Chemical Engineering) |
|CHE311C : MASS TRANSFER-I LAB |
|L |T |P |Credits | |Class Work |: |25 Marks |
|- |- |2 |1 | |Examination |: |75 Marks |
| | | | | |Total |: |100 Marks |
| | | | | |Duration of Examination |: |3 Hours |
Course Objectives: Mass Transfer lab provides students the first-hand experience of verifying various theoretical concepts learnt in theory course that includes Diffusion, Equilibria, Gas Absorption, Cooling tower
Course Outcomes: Students will be able to:
• Learn how to experimentally verify various theoretical principles.
• Visualize practical implementation of mass transfer equipment.
• Develop experimental skills.
LIST OF PRACTICALS / DEMONSTRATIONS:
1. To study mass transfer of vapor in air from solid surface.
2. To study diffusion of vapor in air from liquid surface.
3. To study Drying rate in rotary drum drier
4. To evaluate HETP & HTU in packed column.
5. To find liquid hold up in packed column.
6. To find gas phase mass transfer coefficient in wetted wall column.
7. To study Air water absorption in packed column.
8. To study cooling tower.
NOTE:
1. The students will be required to perform all the experiments from above list; two more experiments may be performed as per the syllabus of CHE305C.
2. The students will be allowed to use non-programmable scientific calculator. However, sharing/exchange of calculator is prohibited in the examination.
3. Electronics gadgets including Cellular phones are not allowed in the examination.
|B. Tech. Semester – V (Chemical Engineering) |
|CHE 313C : PROFESSIONAL TRAINING-I |
|Duration of Training |Credits | |Class Work |: |100 Marks |
|4-6 weeks |1 | |Total |: |100 Marks |
CONTENTS/DESCRIPTION
Professional Trainings/Projects are educational and career development opportunities, providing practical experience in a field or discipline to achieve the following objectives:
• To expose Technical students to the industrial environment, which cannot be simulated in the classroom and hence, creating competent professionals in the industry.
• To Provide possible opportunities to learn, understand and sharpen the real time technical / managerial skills required in the job.
• To learn to apply the Technical knowledge in real industrial situations.
• To gain experience in writing Technical reports/projects.
• To expose students to the engineer’s responsibilities and ethics.
• To familiarize with various materials, processes, products and their applications along with the relevant aspects of quality control.
• To promote academic, professional and/or personal development.
• To expose the students to future employers.
• To understand the social, economic and administrative considerations that influence the working environment of industrial organizations
• To understand the psychology of the workers and their habits, attitudes and approach to problem solving.
During the summer vacation after 4th semester, students will have to undertake Internship / Innovation / Entrepreneurship related activities for a period of 4-6 weeks strictly in accordance with the guidelines to be issued by the TPO/Department. Students may choose either to work on innovation or entrepreneurial activities resulting in start-up or undergo internship with industry/ NGO’s/ Government organizations/ Micro/ Small/ Medium enterprises to make themselves ready for the industry. Learning at Centre of Excellence established in the institutions, Training programmes organized in IITs/ NITs, Live Projects by Industries and Online Training Programmes to improve industry readiness may also to be considered as internship experience and for the purpose of awarding internship Credits.
Every student is required to prepare a file containing documentary proofs of the activities done by him. He/she will have to submit to the department (1) Student’s Diary / Daily log (2) Professional Training/Project Report in the next semester as and when desired by the department.
Student’s Diary / Daily log
The students should record in the daily training diary the day to day account of the observations, impressions, information gathered and suggestions given, if any. It should contain the sketches & drawings related to the observations made by the students. The daily training diary should be signed after every day by the supervisor(s) and/or Incharge of the section where the student has been working. The diary should also be shown to the Faculty Mentor visiting the industry from time to time and got ratified on the day of his visit.
Professional Training/Project Report
After completion of the Professional Training/Project, the student should prepare a comprehensive report to indicate what he has observed and learnt in the training period. The student may contact Industrial Supervisor/ Faculty Mentor/TPO for assigning special topics and problems and should prepare the final report on the assigned topics.
The evaluation of Professional Training/Project will be done by a departmental committee in the next i.e. 7th semester as per Time Table allocated by the department on the basis of the following criteria:
• Regularity in maintenance of the diary;
• Adequacy, quality and purposeful write-up including drawings, sketches and data recorded;
• Variety and relevance of learning experience;
• Originality;
• Practical applications, relationships with basic theory and concepts taught in the courses; etc.
• Presentation (Quality of content /Effectiveness of presentation/Depth of knowledge and skills, etc.).
|B. Tech. Semester – VI (Chemical Engineering) |
|CHE302C : CHEMICAL REACTION ENGINEERING – II |
|L |T |P |Credits | |Class Work |: |25 Marks |
|3 |1 |- |4 | |Examination |: |75 Marks |
| | | | | |Total |: |100 Marks |
| | | | | |Duration of Examination |: |3 Hours |
Course Objectives: To learn:
• Basic concepts of catalysis.
• Kinetics and mechanistic aspects of catalysts.
• Design and rating of catalytic reactors.
• Design aspects of gas-liquid reactors.
Course Outcomes: Students will be able to:
• Design catalytic reactors.
• Identify regions of mass transfer control and reaction rate control and calculate conversion.
Syllabus contents:
UNIT-I: Introduction to catalysis, classification of catalysts, preparation and physical characteristics of solid catalysts, Concepts of physical adsorption and chemisorption. Kinetics of Fluid-Solid Catalytic Reactions, Rate of Adsorption, Desorption, Surface Reaction, Rate equation in terms of Fluid-Phase Concentrations at the catalyst surface.
UNIT-II: External Diffusion Effects on Heterogeneous reactions: Mass transfer diffusion fundamentals, External resistance to mass transfer, Shrinking Core Model. Kinetics of Catalyst Deactivation.
UNIT-III: Diffusion and reaction in porous catalyst: Diffusion and reaction in spherical catalyst pellets, Internal and Overall Effectiveness factors, mass-transfer and reaction in packed bed, multiphase reactor.
UNIT-IV: Design of Heterogeneous Catalytic reactors: Isothermal & Adiabatic reactors; Non-Isothermal, Non- adiabatic Fixed Bed Reactors; Fluidized Bed Reactors.
.
TEXT BOOKS:
1. Elements of Chemical Reaction Engineering by H. Scott Fogler, 2nd Edition, Prentice Hall 2001.
2. Chemical Reaction Engineering by Octave Levenspiel, 3rd Edition, John Wiley & Sons 2001.
REFERENCE BOOKS:
1. Chemical and Catalytic Reaction Engineering, Carberry, J. J., Dover Books on Chemistry, 2001.
2. Chemical Reactor Analysis and Design Gilbert F. Froment, Kenneth B. Bischoff, Juray De Wilde, John Wiley & Sons, Incorporated, 2010.
NOTE:
1. Part A: Till academic session 2020-2021:
In the semester examination, the examiner will set 08 questions in all selecting two from each unit. The candidates will be required to attempt five questions in all selecting at least one from each unit. All questions will carry equal marks.
Part B: From Academic Session 2021-2022 onwards: For the semester examination, nine questions are to be set by the examiner. Question no. 1, containing 6-7 short answer type questions, will be compulsory & based on the entire syllabus. Rests of the eight questions are to be set by setting two questions from each of the four units of the syllabus. The candidates will be required to attempt five questions in all, selecting one from each unit. All questions will carry equal marks.
2. The students will be allowed to use non-programmable scientific calculator. However, sharing/exchange of calculator is prohibited in the examination.
3. Electronics gadgets including Cellular phones are not allowed in the examination.
|B. Tech. Semester – VI (Chemical Engineering) |
|CHE304C : MASS TRANSFER-II |
|L |T |P |Credits | |Class Work |: |25 Marks |
|3 |1 |- |4 | |Examination |: |75 Marks |
| | | | | |Total |: |100 Marks |
| | | | | |Duration of Examination |: |3 Hours |
Course Objectives: To learn unit Operations based on Mass Transfer.
Course Outcomes: Students will be able to:
• List situations where liquid–liquid extraction might be preferred to distillation.
• Explain the concept of breakthrough in fixed-bed adsorption.
• Design solid liquid extractor
• Design distillation column
Syllabus contents:
UNIT-I: Distillation : Raoult's Law, ideal solutions, x-y and T-x-y diagrams, Flash vaporization and condensation, Batch distillation, Steam distillation, Azeotropes.
UNIT-II: Binary distillation, McCabe Thiele and Ponchon_Savarit Method, Total reflux, Minimum and Optimum reflux ratios, Fenske equation, Multicomponent distillation.
UNIT-III: Liquid-Liquid extraction : Application of liqid-liquid extraction, Liquid Equilibria, Equilateral- Triangular Coordinates, Systems of Three Liquids-One pair partially soluble, Systems of Three Liquids- Two pairs partially soluble, Choice of Solvent, Single stage extraction, Multistage extraction. Extraction Equipment
UNIT-IV: Leaching : Application of leaching, Moving-bed leaching, Dispersed-solid leaching, Single stage leaching, Multistage leaching. Leaching Equipment. Adsorption : Types of Adsorption, Adsorption Isotherms, Single stage adsorption, Multistage adsorption, Adsorption Equipment.
TEXT BOOKS:
1. Binay K.Dutta, Principles of Mass Transfer and Separation Processes, 2nd edition, Prentice Hall of India,2007.
2. R.E.Treybal, Mass Transfer Operations, 3rd Edition, McGraw Hill, New Delhi, 1983.
3. W.L. McCabe, J. Smith and P. Harriot, Unit Operations of Chemical Engineering, 7th Edition, Tata McGraw Hill, India, 2014.
REFERENCE BOOKS:
1. C.J. Geankoplis, Transport Processes and Unit Operations, 3rd Edition, Prentice Hall, India, 1993.
2. A.S. Foust, Principles of Unit Operations, 2nd Edition, Wiley, New York, 1980.
NOTE:
1. Part A: Till academic session 2020-2021:
In the semester examination, the examiner will set 08 questions in all selecting two from each unit. The candidates will be required to attempt five questions in all selecting at least one from each unit. All questions will carry equal marks.
Part B: From Academic Session 2021-2022 onwards: For the semester examination, nine questions are to be set by the examiner. Question no. 1, containing 6-7 short answer type questions, will be compulsory & based on the entire syllabus. Rests of the eight questions are to be set by setting two questions from each of the four units of the syllabus. The candidates will be required to attempt five questions in all, selecting one from each unit. All questions will carry equal marks.
2. The students will be allowed to use non-programmable scientific calculator. However, sharing/exchange of calculator is prohibited in the examination.
3. Electronics gadgets including Cellular phones are not allowed in the examination.
|B. Tech. Semester – VI (Chemical Engineering) |
|CHE306C : PROCESS CONTROL |
|L |T |P |Credits | |Class Work |: |25 Marks |
|3 |1 |- |4 | |Examination |: |75 Marks |
| | | | | |Total |: |100 Marks |
| | | | | |Duration of Examination |: |3 Hours |
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Course Objectives:To introduce the fundamentals of process control with applications using P, PI, and PID controllers. The course will teach the students about mathematical models based on transfer function approach for single loop systems, how to obtain dynamic response of open loop and closed loop systems, stability analysis in transient and frequency domains, and controller tuning methods. The course would end with more advanced concepts like feed-forward control, ratio control, model- predictive control, ratio control, dead-time compensation etc.
Course Outcomes: Students will be able to understand the importance of process dynamics (unsteady state operation), Tune a controller to reject disturbances or manage operating point transitions.
[pic]
Syllabus Contents:
UNIT-I : Introductory Concepts: Need for control and automation, control logic, servo and regulatory control, block diagrams, control structures (feedback vs. feed forward), process and instrumentation diagrams. Laplace transforms, solution of ODEs using Laplace transform.
Transfer function approach, response of first order systems: step, impulse and sinusoidal response,first order systems in series.
UNIT-II: Second order systems, higher order systems, transportation lag and dead time.
Linear closed loop systems, development of block diagrams, classical feedback controllers.
Final control element (control valves), block diagram reduction techniques, closed loop response, servo and regulatory problems.
UNIT-III: Stability analysis, Routh stability criterion, Root locus diagrams (rule based), Introduction tofrequency response, notion of stability, Bode diagrams, Bode stability criterion.
UNIT-IV : Nyquist plots, Nyquist stability criterion
Controller tuning: Ziegler-Nichols method, Cohen-Coon method.
Introduction to advanced controllers: cascade control, feed forward control, ratio control, Smith-Predictor, dead time compensation.
TEXT BOOKS:
1. Coughanowr, D. R., LeBlanc, S. “Process Systems Analysis and Control”, 3rd edition, McGraw-Hill (2008).
REFERENCES BOOKS:
1. Seborg, D.E., Edgar, T.F., Mellichamp, D.A. “Process Dynamics and Control”, 2nd edition, John Wiley.
2. Stephanopoulos, G. “Chemical Process Control: An Introduction to Theory and Practice”, Pearson Education.
NOTE:
1. Part A: Till academic session 2020-2021:
In the semester examination, the examiner will set 08 questions in all selecting two from each unit. The candidates will be required to attempt five questions in all selecting at least one from each unit. All questions will carry equal marks.
Part B: From Academic Session 2021-2022 onwards: For the semester examination, nine questions are to be set by the examiner. Question no. 1, containing 6-7 short answer type questions, will be compulsory & based on the entire syllabus. Rests of the eight questions are to be set by setting two questions from each of the four units of the syllabus. The candidates will be required to attempt five questions in all, selecting one from each unit. All questions will carry equal marks.
2. The students will be allowed to use non-programmable scientific calculator. However, sharing/exchange of calculator is prohibited in the examination.
3. Electronics gadgets including Cellular phones are not allowed in the examination.
|B. Tech. Semester – V (Chemical Engineering) |
|CHE308C : EQUIPMENT DESIGN |
|L |T |P |Credits | |Class Work |: |25 Marks |
|3 |- |- |3 | |Examination |: |75 Marks |
| | | | | |Total |: |100 Marks |
| | | | | |Duration of Examination |: |3 Hours |
Course Objectives: To study the concepts of Process vessels, their Materials mechanics, pressure vessel design, Tall Tower Design, selection and design of closures, Heat Exchangers.
Course Outcomes: Students will be:
• Able to design Pressure vessels, Heat exchangers.
• Familiar with design and basic concepts of equipments such as Pressure vessels, Heat exchangers, supports, Tall Tower and storage vessels.
Syllabus contents:
UNIT-I: Mechanics of Materials: Stress, strain, Biaxial and tri-axial stress, Stress-strain relationship for elastic bodies, Theories of failure, Thermal stresses, Torsion of solid and hollow cylindrical shafts, Thin and thick cylinders.
UNIT-II: Pressure Vessel: Introduction of codes for pressure vessel design, classification of pressure vessels, Design of cylindrical and spherical shells under internal and external pressure, selection and design of closures, optimum length to diameter ratio of pressure vessel using common types of closures.
UNIT-III: Design of jacketed portion of vessels, Selection and design of nozzles, Elementary idea of compensation for openings, Selection of gaskets, selection and design of flanges, pipe thickness calculation under internal and external pressure. Complete design calculations and shop drawing for at least one pressure vessel using heads and flanges as per code specifications.
UNIT-IV: Tall Tower Design: Design of shell, skirt, bearing plate and anchor bolts used at high wind and seismic conditions. Supports: Design of lug support and saddle support including bearing plates and anchor bolts. Storage Tanks: Filling and breathing losses, classification of storage tanks, Design of liquid and gas storage tanks.
TEXT BOOKS:
1. Process Equipment Design: L.E. Brownell and H.E. Loung- John Wiley, New Delhi.
2. Introduction of Chemical Equipment Design: B.C. Bhattacharya -Chemical Engineering Education Development Centre, IIT, Madras.
3. Process Equipment Design: M.V. Joshi and V.V. Mahagani Macmillan India Ltd.
REFERENCE BOOKS:
1. Code for unfired pressure vessels: IS: 2825-1969-ISI, New Delhi.
NOTE:
1. Part A: Till academic session 2020-2021:
In the semester examination, the examiner will set 08 questions in all selecting two from each unit. The candidates will be required to attempt five questions in all selecting at least one from each unit. All questions will carry equal marks.
Part B: From Academic Session 2021-2022 onwards: For the semester examination, nine questions are to be set by the examiner. Question no. 1, containing 6-7 short answer type questions, will be compulsory & based on the entire syllabus. Rests of the eight questions are to be set by setting two questions from each of the four units of the syllabus. The candidates will be required to attempt five questions in all, selecting one from each unit. All questions will carry equal marks.
2. The students will be allowed to use non-programmable scientific calculator. However, sharing/exchange of calculator is prohibited in the examination.
3. Electronics gadgets including Cellular phones are not allowed in the examination.
|B. Tech. Semester – VI (Chemical Engineering) |
|CHE350C : NANOSCIENCE FOR CHEMICAL ENGINEERS |
|L |T |P |Credits | |Class Work |: |25 Marks |
|3 |- |- |3 | |Examination |: |75 Marks |
| | | | | |Total |: |100 Marks |
| | | | | |Duration of Examination |: |3 Hours |
Course Objectives: To instruct the student in the engineering, physics, chemistry, biology and exciting applications in the fields of nanoscience and nanotechnology.
Course Outcomes: The student shall be able to understand the novelty offered by nanotechnologies in diverse areas of human endeavors and engineering applications along with the science behind those applications.
Syllabus contents:
UNIT-I: Materials and their Structures: Introduction to materials and their types, bonding in materials; crystal structures and defects; amorphous materials; origins of properties of materials; Effect of nanostructures on properties of materials
UNIT-II: Nano Measurement and Engineering: AFM; STM; Types of nanostructures; 0, 1 and 2 dimensional nanostructures. Biomaterials and nano-biotechnology, Characterization of phases and quantification of phases, Bandgap engineering
UNIT-III: Design and Synthesis: Synthesis of Nanomaterials, Applications of Nanomaterials: In textile industry, in catalytic operations, in energy generation, in energy storage, in environmental remediation and in sensors and devices Molecular motors application; MEMS and NEMS devices.
UNIT-VI: Laboratory synthesis: Magnetic Nanomaterials, undoped and doped semi conduct nanomaterials, ferroelectric nanomaterials, chemical, Sol gel & hydrothermal synthesis of nanomaterials
TEXT BOOKS:
1. Introduction to Nanoscience, S.M. Lindsay, Oxford University Press, 2010, ISBN: 978–019–954421–9 (Pbk).
2. Nanoscience, Hans-Eckhardt Schaefer, Springer, 2010, ISBN 978-3-642-10558-6.
REFERENCE BOOKS:
1. NANO: The Essentials Understanding Nanoscience and Nanotechnology, T. Pradeep, Tata McGraw Hill Publishing Company Limited, 2007, 0-07-154830-0.
2. Textbook of Nanoscience and Nanotechnology, Authors: Murty, B.S., Shankar, P., Raj, B., Rath, B.B., Murday, J. ISBN 978-3-642-28029-0, Publisher Springer-Verlag Berlin Heidelberg
NOTE:
1. Part A: Till academic session 2020-2021:
In the semester examination, the examiner will set 08 questions in all selecting two from each unit. The candidates will be required to attempt five questions in all selecting at least one from each unit. All questions will carry equal marks.
Part B: From Academic Session 2021-2022 onwards: For the semester examination, nine questions are to be set by the examiner. Question no. 1, containing 6-7 short answer type questions, will be compulsory & based on the entire syllabus. Rests of the eight questions are to be set by setting two questions from each of the four units of the syllabus. The candidates will be required to attempt five questions in all, selecting one from each unit. All questions will carry equal marks.
2. The students will be allowed to use non-programmable scientific calculator. However, sharing/exchange of calculator is prohibited in the examination.
3. Electronics gadgets including Cellular phones are not allowed in the examination.
|B. Tech. Semester – VI (Chemical Engineering) |
|CHE352C : RENEWABLE ENERGY |
|L |T |P |Credits | |Class Work |: |25 Marks |
|3 |- |- |3 | |Examination |: |75 Marks |
| | | | | |Total |: |100 Marks |
| | | | | |Duration of Examination |: |3 Hours |
Course Objectives: Basic concepts of renewable energy, Energy utilization, technical and social implications. Different types of Renewable Energy resources, New Energy Sources, Hydrogen storage.
Course Outcomes: Students will be:
• Able to understand Energy Conversion technologies, Wind Energy, principles of power generation, solar energy.
• Familiar with Solar heating devices, photovoltaic systems, Biomass and Biofuels, Geothermal energy, tidal energy, Wave energy etc.
Syllabus contents:
UNIT-I: Principles of renewable energy, Energy utilization, Fundamentals, scientific principles, technical and social implications. Renewable Energy resources and their potential, Energy Conversion technologies. Wind Energy, Wind mill and turbine, Wind Power plant, classification and principles of power generation, site selection, Wind energy applications and new developments.
UNIT-II: Solar radiation: Extraterrestrial solar radiation, estimation of solar radiation. Solar heating devices: Solar water heater: sheltered and unsheltered heaters, systems with separate storage, selective surfaces, solar ponds, solar concentrators and other devices. Silicon cell, photon absorption, cell efficiency, solar cell construction, types and usage of photovoltaic systems.
UNIT-III: Biomass and Biofuels: Biofuel classification, combustion, pyrolysis, biomass gasification and other thermo-chemical processes, production of alcohol and biogas, biogas plants and types. Transesterification of vegetable oils for biodiesel production, characterization of biodiesel, economics, current trends, and future prospects in usage of biodiesel.
UNIT-IV: New Energy Sources: Geothermal energy, Wave energy, tidal energy, Ocean thermal energy, small hydel power, agriculture residues, Hydrogen Energy: Hydrogen energy system and analysis, hydrogen production: Electrolysis, thermo-chemical, Hydrogen from fossil fuel.
Hydrogen storage: Carbon storage materials: cryogenic hydrogen storage, hydrogen fuel cells.
TEXT / REFERENCE BOOKS:
1. R K Singhal, Non-conventional energy sources , S K Kataria& Sons, Darya Ganj, New Delhi.
2. D S Chauhan, S K Srivastava, "Non Conventional energy resources", New Age International (P) limited.
3. D Mukherjee, S Chakrabarti, "Fundamentals of Renewable Energy", New Age International (P) limited.
NOTE:
1. Part A: Till academic session 2020-2021:
In the semester examination, the examiner will set 08 questions in all selecting two from each unit. The candidates will be required to attempt five questions in all selecting at least one from each unit. All questions will carry equal marks.
Part B: From Academic Session 2021-2022 onwards: For the semester examination, nine questions are to be set by the examiner. Question no. 1, containing 6-7 short answer type questions, will be compulsory & based on the entire syllabus. Rests of the eight questions are to be set by setting two questions from each of the four units of the syllabus. The candidates will be required to attempt five questions in all, selecting one from each unit. All questions will carry equal marks.
2. The students will be allowed to use non-programmable scientific calculator. However, sharing/exchange of calculator is prohibited in the examination.
3. Electronics gadgets including Cellular phones are not allowed in the examination.
|B. Tech. Semester – VI (Chemical Engineering) |
|CHE354C : POLYMER SCIENCE AND ENGINEERING |
|L |T |P |Credits | |Class Work |: |25 Marks |
|3 |- |- |3 | |Examination |: |75 Marks |
| | | | | |Total |: |100 Marks |
| | | | | |Duration of Examination |: |3 Hours |
Course Objectives: Basic concepts of Polymerization Reactions, Polymer Blends, Polymerization Processes, Molecular Weight Estimation methods, Rheology, Moulding and Casting Techniques.
Course Outcomes: Students will be:
• Able to understand different polymerization processes and their kinetics, Polymer degradation, Rheological studies.
• Familiar with polymer additives and blends, Polymerisation techniques, Calendering, Moulding and Casting Technique, applications of polymers in different fields.
Syllabus contents:
UNIT-I: Chemistry of Polymerization Reactions- Functionality, Polymerization reactions, polycondensation, addition, free radical and chain polymerization. Copolymerization, block and graft polymerizations, stereo specific polymerization. Polymer Blends.
UNIT-II: Polymerization Kinetics- Kinetics of radical, Chain and ionic polymerisation and copolymerization systems. Polymerisation Processes - Bulk, Solution, Emulsion and suspension polymerisation, Q-e Scheme, Spherulites, Additives.
UNIT-III: Molecular Weight Estimation -Average molecular weight: number average and weight average. Theoretical distributions, methods for the estimation of molecular weight. Characterization and Analysis of Polymer: Polymer degradation, Membrane Osmometry ,Thermal Analysis and other methods.
Rheology:- simple rheological response, simple linear viscoelastic models- Maxwell. Voigot, material response time, temperature dependence of viscosity. Rheological studies.
UNIT-IV: Processing methods, Mixing including internal mixture, Calendering, Extrusion, Moulding Technique, Forming Technique, Casting, Thermoforming, Applications of polymers in different fields.
TEXT BOOKS:
1. Text Book of Polymer Science: Jr. Billmayer & W. Fred- Wiley Tappers.
2. Polymer Science: Shreedhar & Gowarikar.
3. Polymer Science & Technology: Premamoy Ghosh, Tata Mc Graw Hill.
4. Polymer Chemistry- An Introduction: Malcolm P. Stevens.
REFERENCE BOOKS:
1. Principles of Polymers systems: Rodringuez- Tata Mc Graw Hill.
2. Polymer Processing: J.M. Mc kelvey -John wiley.
3. Polymer Science and Engineering: Davil J. Williams- Prentice Hall of India, New Delhi.
NOTE:
1. Part A: Till academic session 2020-2021:
In the semester examination, the examiner will set 08 questions in all selecting two from each unit. The candidates will be required to attempt five questions in all selecting at least one from each unit. All questions will carry equal marks.
Part B: From Academic Session 2021-2022 onwards: For the semester examination, nine questions are to be set by the examiner. Question no. 1, containing 6-7 short answer type questions, will be compulsory & based on the entire syllabus. Rests of the eight questions are to be set by setting two questions from each of the four units of the syllabus. The candidates will be required to attempt five questions in all, selecting one from each unit. All questions will carry equal marks.
2. The students will be allowed to use non-programmable scientific calculator. However, sharing/exchange of calculator is prohibited in the examination.
3. Electronics gadgets including Cellular phones are not allowed in the examination.
|B. Tech. Semester – VI (Chemical Engineering) |
|CHE356C : ADVANCED SEPARATION PROCESSES |
|L |T |P |Credits | |Class Work |: |25 Marks |
|3 |- |- |3 | |Examination |: |75 Marks |
| | | | | |Total |: |100 Marks |
| | | | | |Duration of Examination |: |3 Hours |
Course Objectives:
• To familiarize students with various advanced aspects of separation processes and the selection of separation processes.
• To enable students to understand the principles and processes of membrane separation and chromatography and to design a membrane unit to achieve a specified separation.
• To introduce them to new trends used in the separation technologies.
Course Outcomes:
At the end of the course, the student will be able to:
• Explain membrane processes in terms of the membrane, feed, sweep, retentate, permeate, and solute membrane interactions. Distinguish among microfiltration, ultrafiltration,nanofiltration, virus filtration, sterile filtration, filter-aid filtration, and reverse osmosis interms of average pore size. Explain common idealized flow patterns in membrane modules.
• Understand surface properties based separation processes, ion exchange and chromatographic methods.
Syllabus contents:
UNIT-I: Fundamentals; membrane based separation processes.Membrane Separation: Characteristics of organic and inorganicmembranes, basis ofmembrane selection, osmotic pressure, partitioncoefficient and permeability, concentrationpolarization, electrolytediffusion and facilitated transport, macro-filtration, ultra-filtration and nano-filtration.
UNIT-II: Reverse osmosis, electro-dialysis, and Industrial applications. External field induced membrane separation processes for colloidal particles; gas separation.
UNIT-III: Surfactant based separation processes; Bubble and Foam Fractionation: Nature of bubbles and foams, stability of foams, foam fractionation techniques, batch, continuous, single stage and multistage columns.
Centrifugal separation processes.
UNIT-IV: Ion exchange and Chromatographic Methods of Separation: Gel, solvent, ion and highperformance liquidchromatography; supercritical fluid extraction.
TEXT BOOKS:
1. King C.J., “Separation Processes”, Tata McGraw Hill. 1982.
2. Nakagawal, O. V., “Membrane Science and Technology”, Marcel Dekker, 1992.
3. Humphrey, J and G. Keller, Separation Process Technology, McGraw-Hill, 1997.
4. Khoury F.M., “Multistage Separation Processes”, 3rdEd., CRC Press. 2004.
REFERENCE BOOKS:
1. Wankat P.C., “Separation Process Engineering”, 2ndEd., Prentice Hall.2006.
2. Seader J.D. and Henley E.J., “Separation Process Principles”, 2ndEd.,Wiley2006.
3. Basmadjian D., “Mass Transfer and Separation Processes: Principles and Applications”, 2ndEd.,CRC Press.2007.
4. Phillip C. Wankat, Separation Process Engineering (2ndEdition),Printice Hall,2007.
5. Rousseau, R. W., “Handbook of Separation Process Technology”, John Wiley, New York, 2009.
|B. Tech. Semester – VI (Chemical Engineering) |
|CHE310C : CHEMICAL REACTION ENGINEERING LAB |
|L |T |P |Credits | |Class Work |: |25 Marks |
|- |- |2 |1 | |Examination |: |75 Marks |
| | | | | |Total |: |100 Marks |
| | | | | |Duration of Examination |: |3 Hours |
Course Objectives: Chemical Reaction Engineering lab provides the opportunity to the students for verifying various theoretical concepts learnt in theory courses. It also serves as a bridge between theory and practice. Students will learn to:
• Calculate rate, rate constant, activation energy and order of reaction.
• Interpret kinetic data to find order of reactions.
• Operate different reactors efficiently using basic knowledge about their functioning.
Course Outcomes: Students will be able to:
• Analyze and interpret given reaction rate data using various methods.
• Compare the effect of residence time on conversion for CSTR and PFR.
• Use the experimental kinetic data for reactor design.
LIST OF PRACTICALS / DEMONSTRATIONS:
1. To study the kinetics of reaction adiabatically in a batch reactor.
2. To find the Arrhenius constant.
3. Study the kinetics of reaction for all the combination of the given three CSTR in series.
4. RTD Study of the given three CSTR in series (Pulse Input).
5. RTD Study of the given three CSTR in series (Step Input).
6. Study the kinetics of reaction for Plug Flow Reactor.
7. RTD Study of the Plug Flow Reactor (Pulse Input).
8. RTD Study of the Plug Flow Reactor (Step Input).
9. Adsorption study of Heavy metal / Dye on activated Carbon.
10. Adsorption study of oxalic acid on activated Carbon.
11. Study the effect of surface area on adsorption.
12. To study the performance of a fluidized bed reactor.
NOTE:
1. The students will be required to perform the 06 experiments from above list; remaining two experiments may either be performed from the above list or designed and set by the Dept. as per the scope of the syllabus of CHE-301C.
2. The students will be allowed to use non-programmable scientific calculator. However, sharing/exchange of calculator is prohibited in the examination.
3. Electronics gadgets including Cellular phones are not allowed in the examination.
|B. Tech. Semester – VI (Chemical Engineering) |
|CHE312C : MASS TRANSFER-II LAB |
|L |T |P |Credits | |Class Work |: |25 Marks |
|- |- |2 |1 | |Examination |: |75 Marks |
| | | | | |Total |: |100 Marks |
| | | | | |Duration of Examination |: |3 Hours |
Course Objectives: This particular lab focuses on Distillation, Adsorption, Leaching, LLE, drying.
Course Outcomes: Students will be able to:
• Learn how to experimentally verify various theoretical principles.
• Visualize practical implementation of chemical engineering equipment.
• Develop experimental skills.
LIST OF PRACTICALS / DEMONSTRATIONS:
1. To study Raylieh equation for batch distillation
2. To find vapor- liquid equation data.
3. To study batch distillation with reflux.
4. To study adsorbtion isotherm.
5. To study kinetics of adsorption.
6. To study solid- liquid extraction.
7. To study liquid- liquid extraction in packed column.
NOTE:
1. The students will be required to perform all the experiments from above list as per the syllabus of CHE304C.
2. The students will be allowed to use non-programmable scientific calculator. However, sharing/exchange of calculator is prohibited in the examination.
3. Electronics gadgets including Cellular phones are not allowed in the examination.
|B. Tech. Semester – VII (Chemical Engineering) |
|CHE314C : INSTRUMENTATION & CONTROL LAB |
|L |T |P |Credits | |Class Work |: |25 Marks |
|- |- |2 |1 | |Examination |: |75 Marks |
| | | | | |Total |: |100 Marks |
| | | | | |Duration of Examination |: |3 Hours |
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Course Objectives: Objective of the course is to introduce the basics of instrumentation and process control through a hands-on practical experience. Principles of operation of different measuring devices for temperature, level, pressure, flow, pH, humidity, density, and viscosity will be introduced to impart knowledge of transmitters, transducers, converters, control valves, digital and analog components related to PLC, DCS, SCADA systems.
Course Outcomes: Students will be well-familiar with instrumentation and automation as relevant to modern chemical plant operation.
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LIST OF EXPERIMENTS:
Modeling and Simulation of Chemical Engineering Systems like:
1. Liquid Level Tank (Non-interacting system).
2. Liquid Level Tank (Interacting system).
3. Time constant of a Mercury Thermometer.
4. Pressure control system trainer.
5. Temperature control system trainer.
6. Level control system trainer.
7. Flow control system trainer.
8. Ratio control system trainer
9. Analysis of Valve.
10. Temperature and pressure measuring devices.
11. Level and flow measuring devices.
12. Viscosity and pH measuring devices.
13. Transmitters and transducers.
14. Flow-level cascade controls.
TEXT BOOKS:
1. William C. Dunn, Fundamentals of Industrial Instrumentation and Process Control, Mc- GrawHill (2005).
2. S.K. Singh, Industrial Instrumentation and Control, 3rd edition, McGraw-Hill (2008).
3. As per manuals/literature supplied by Software Vendor.
REFERENCE BOOKS:
1. Seborg, D.E., Edgar, T.F., Mellichamp, D.A. “Process Dynamics and Control”, 2nd edition, John Wiley (2003).
2. Stephanopoulos, G. “Chemical Process Control: An Introduction to Theory and Practice”, Pearson Education (1984).
NOTE:
1. The students will be required to perform the 08 experiments from above list as designed and set by the Dept. as per the scope of the syllabus of CHE306C.
2. The students will be allowed to use non-programmable scientific calculator. However, sharing/exchange of calculator is prohibited in the examination.
3. Electronics gadgets including Cellular phones are not allowed in the examination.
|Open Elective-II |
|CHE457C : INDUSTRIAL SAFTEY |
|L |T |P |Credits | |Class Work |: |25 Marks |
|3 |- |- |3 | |Examination |: |75 Marks |
| | | | | |Total |: |100 Marks |
| | | | | |Duration of Examination |: |3 Hours |
Course Objectives: The purpose of this course is
• To teach the students the concept of industrial safety and provide useful practical knowledge for workplace safety.
• To identify, evaluate control the hazards to prevent or mitigate harm or damage to people, property and the environment.
• To aware students about the safety aspects in various industries.
Course Outcomes: Students will be able to:
• Identify hazard areas and develop safety programs to prevent the damage or loss
• Assess safety practices and programs
• Conduct safety audits and improve safety practices. .
Syllabus contents:
UNIT-I: Introduction: Concept of loss prevention, origin of process hazards, types of process hazards, acceptable risks, accident and loss statics, nature of accident process, concepts of inherent safety in plants or Factories, dose Vs response curve, toxicants entry route, thresh limit values, safety regulations.
UNIT-II: Hazards: Fire, Chemical (industrial and laboratory scale), electrical, mechanical, biohazards (natural and anthropogenic), toxic materials, their types and preventive measures, Liquid and vapor phase hazardous methods, storage and handling, containment, precautions, Personal safety precautions.
UNIT-III: Risk management principles, risk analysis techniques, risk control, hazards operability studies, hazard analysis, Fault tree analysis, Consequences analysis, human error analysis, accidental error analysis, economics of risk management, check list, reliability theory, event tree, HAZOP, safety reviews, what if analysis.
UNIT-IV: Safety audit, procedure for safety auditing, audit report, safety report, safety training, emergency planning and disaster management, introduction to security risk factors tables.
TEXT BOOKS:
1. Chemical Hazards and safety, 2nd Edition, Dawande Denet & Co. , 2012
2. Loss preventions in process industries, Lees Butterworth-Heinemann, 1980.
3. Industrial safety Handbook, William and Handley, McGraw Hill.
REFERENCE BOOKS:
1. Safety and Hazard management in Chemical Industries, Vyas, Atlantic 2013.
2. Industrial safety, health environment & Security, Basudev Panda, Laxmi publication ISBN- 97893-81159-43-9
3. Industrial Safety and Health Management, 4th Edition, C. Ray Asfahl, Prentice Hall International Series, 1984
4. Industrial Accident Prevention : A Safety Management Approach, Herbert William Heinrich
NOTE:
1. Part A: Till academic session 2020-2021:
In the semester examination, the examiner will set 08 questions in all selecting two from each unit. The candidates will be required to attempt five questions in all selecting at least one from each unit. All questions will carry equal marks.
Part B: From Academic Session 2021-2022 onwards: For the semester examination, nine questions are to be set by the examiner. Question no. 1, containing 6-7 short answer type questions, will be compulsory & based on the entire syllabus. Rests of the eight questions are to be set by setting two questions from each of the four units of the syllabus. The candidates will be required to attempt five questions in all, selecting one from each unit. All questions will carry equal marks.
2. The students will be allowed to use non-programmable scientific calculator. However, sharing/exchange of calculator is prohibited in the examination.
3. Electronics gadgets including Cellular phones are not allowed in the examination.
|Open Elective-III |
|CHE459C : NANOSCIENCE AND NANOTECHNOLOGY |
|L |T |P |Credits | |Class Work |: |25 Marks |
|3 |- |- |3 | |Examination |: |75 Marks |
| | | | | |Total |: |100 Marks |
| | | | | |Duration of Examination |: |3 Hours |
Course Objectives: To instruct the student in the engineering, physics, chemistry, biology and exciting applications in the fields of nanoscience and nanotechnology.
Course Outcomes: The student shall be able to understand the novelty offered by nanotechnologies in diverse areas of human endeavors and engineering applications along with the science behind those application.
Syllabus contents:
UNIT-I: Types of materials; bonding in materials; crystal structures and defects; amorphous materials; origins of properties of materials; Effect of nanostructures on properties of materials.
The science of materials – materials science; Historical use of nanoparticles; discovery of the carbon nanotubes; fullerenes; nanostructured materials
UNIT-II: Particle-wave duality; de-Broglie waves; Schrodinger equation in 1-Dimension; Superposition; Energy eigenstates; Interpretation of wave function; Fermions and Bosons; Electron density of states; Energy bandgaps; Fermi energy; Excitons and Bohr radius.
UNIT-III: AFM; STM; Transport in nanostructures; 0,1 and 2 dimensional nanostructures; Bandgap engineering; Molecular motors; MEMS and NEMS devices. Biomaterials and nano-biotechnology.
UNIT-IV: Synthesis of Nanomaterials – ZnO and Fe3O4. Characterization of phases and quantification of phases. Applications of Nanomaterials: In textile industry, in catalytic operations, in energy generation, in energy storage, in environmental remediation and in sensors and devices.
TEXT BOOKS:
1. NANO:The Essentials Understanding Nanoscience and Nanotechnology, T. Pradeep, Tata McGraw Hill
Publishing Company Limited, 2007, 0-07-154830-0.
2. Material Science and Engineering, 7th ed. , William D. Callister, Johan Wiley & Sons, Inc.
3. Nanostructured Materials and Nanotechnology, Hari Singh Nalwa, Academic Press, 2002.
4. Nanostructures and Nanomaterials, synthesis, properties and applications., Guozhong Cao, Imperial College Press, 2004.
REFERENCE BOOKS:
1. Introduction to Nanoscience, S.M. Lindsay, Oxford University Press, 2010, ISBN: 978–019–954421–9 (Pbk).
2. Nanoscience, Hans-Eckhardt Schaefer, Springer, 2010, ISBN 978-3-642-10558-6.
3. Chemistry of nanomaterials: Synthesis, Properties and applications. C.N.R. Rao, Achim Muller, A.K. Cheetham, Wiely-VCH, 2004.
NOTE:
1. Part A: Till academic session 2020-2021:
In the semester examination, the examiner will set 08 questions in all selecting two from each unit. The candidates will be required to attempt five questions in all selecting at least one from each unit. All questions will carry equal marks.
Part B: From Academic Session 2021-2022 onwards: For the semester examination, nine questions are to be set by the examiner. Question no. 1, containing 6-7 short answer type questions, will be compulsory & based on the entire syllabus. Rests of the eight questions are to be set by setting two questions from each of the four units of the syllabus. The candidates will be required to attempt five questions in all, selecting one from each unit. All questions will carry equal marks.
2. The students will be allowed to use non-programmable scientific calculator. However, sharing/exchange of calculator is prohibited in the examination.
3. Electronics gadgets including Cellular phones are not allowed in the examination.
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