Multisamplers Agilent InfinityLab LC Series User Manual

Multisamplers

Agilent InfinityLab LC Series

User Manual

Agilent InfinityLab LC Series Multisamplers User Manual

Notices

Document Information

Document No: SD-29000238 Rev. H Edition: 04/2021

Copyright

? Agilent Technologies, Inc. 2014-2021

No part of this manual may be reproduced in any form or by any means (including electronic storage and retrieval or translation into a foreign language) without prior agreement and written consent from Agilent Technologies, Inc. as governed by United States and international copyright laws.

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The material contained in this document is provided "as is," and is subject to being changed, without notice, in future editions. Further, to the maximum extent permitted by applicable law, Agilent disclaims all warranties, either express or implied, with regard to this manual and any information contained herein, including but not limited to the implied warranties of merchantability and fitness for a particular purpose. Agilent shall not be liable for errors or for incidental or consequential damages in connection with the furnishing, use, or performance of this document or of any information contained herein. Should Agilent and the user have a separate written agreement with warranty terms covering the material in this document that conflict with these terms, the warranty terms in the separate agreement shall control.

Technology Licenses

The hardware and/or software described in this document are furnished under a license and may be used or copied only in accordance with the terms of such license.

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Safety Notices

CAUTION

A CAUTION notice denotes a hazard. It calls attention to an operating procedure, practice, or the like that, if not correctly performed or adhered to, could result in damage to the product or loss of important data. Do not proceed beyond a CAUTION notice until the indicated conditions are fully understood and met.

WARNING

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Agilent InfinityLab LC Series Multisamplers User Manual

In This Guide

This manual covers the following InfinityLab LC Series Multisamplers: ? Agilent 1290 Infinity II Multisampler (G7167B), ? Agilent 1260 Infinity II Multisampler (G7167A), ? Agilent 1290 Infinity II Bio Multisampler (G7137A), and ? Agilent 1260 Infinity II Bio-Inert Multisampler (G5668A)

1 Introduction

This chapter gives an introduction to the Multisampler.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical and performance specifications.

3 Using the Module

This chapter explains the essential operational parameters of the module.

4 Preparing the Module

This chapter explains the operational parameters of the module.

5 Optimizing Performance

This chapter gives hints on how to optimize the performance or use additional devices.

6 Troubleshooting and Diagnostics

This chapter gives an overview about the troubleshooting and diagnostic features and the different user interfaces.

7 Error Information

This chapter describes the meaning of error messages, and provides information on probable causes and suggested actions how to recover from error conditions.

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8 Test Functions and Calibration

This chapter describes the built in test functions.

9 Maintenance

This chapter describes the maintenance of the Multisampler

10 Parts for Maintenance and Upgrade or Options

This chapter provides information on parts material required for the module.

11 Identifying Cables

This chapter provides information on cables used with the modules.

12 Hardware Information

This chapter describes the module in more detail on hardware and electronics.

13 LAN Configuration

This chapter provides information on connecting the detector to the Agilent ChemStation PC.

14 Appendix

This chapter provides addition information on safety, legal and web.

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Contents

1 Introduction 11

Product Description (G7167B) 12 Features (G7167B) 13 Product Description (G7167A) 14 Features (G7167A) 15 Product Description (G5668A) 16 Features (G5668A) 17 Product Description (G7137A) 18 Features (G7137A) 19 Overview of the Module 20 Standard Single Needle Setup 22 Injection Sequences 24 System Overview 33

2 Site Requirements and Specifications 41

Site Requirements 42 Physical Specifications 46 Performance Specifications 50 Specifications of the Sample Cooler 58 Specifications of the Sample Thermostat 60

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3 Using the Module 62

Magnets 63 Turn on/off 64 Status indicators 66 Drawer Status Indicator 67 Insert vial trays/wellplates 68 Remove vial trays/wellplates 69 Installing the Optional Sample Cooler/Thermostat 70 Using the Optional Sample Cooler/Sample Thermostat 78 Transporting the Sampler 88 Solvent Information 93 Reset the Multisampler in Case of an Error 105 Agilent Local Control Modules 108

4 Preparing the Module 109

Leak and Waste Handling 110 Preparing the Multisampler 111 Recommended Mats and Vials 113 Configure Well Plate Types 116 Capillary Coding Guide 119 Installing Capillaries 121 Flow Connections to the Washport (Standard) 126 Flow Connections to the Washport (Dual-Needle) 128 Installing the Bypass Capillary (Dual Needle) 130 Flow Connections to the Washport (Multiwash) 133 Setting up the Autosampler with Agilent OpenLab CDS ChemStation Edition 135 Setting up the Dual Needle System with Agilent OpenLAB CDS ChemStation Edition 143

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5 Optimizing Performance 157

Delay Volume and Extra-Column Volume 158 How to Configure the Optimum Delay Volume 159 How to Achieve Higher Injection Volumes 163 How to Achieve High Throughput 165 How to Achieve Higher Resolution 166 How to Achieve Higher Sensitivity 169 How to Achieve Lowest Carryover 170

6 Troubleshooting and Diagnostics 172

User Interfaces 173 Agilent Lab Advisor Software 174

7 Error Information 175

What Are Error Messages 177 General Error Messages 178 Sampler Error Messages 186 Sample Cooler/Sample Thermostat Error Messages 198

8 Test Functions and Calibration 204

Introduction 205 System Pressure Test 206 Auto Referencing 209 Maintenance Positions 211 Injector Steps 215 Sample Cooler Function Test 217 Sampler Leak Test 218

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9 Maintenance 219

Introduction to Maintenance 220 Warnings and Cautions 222 Overview of Maintenance 224 Clean the Module 225 Removal and Installation of the Front Door 226 Remove the Needle Assembly 229 Install the Needle Assembly 234 Exchange the Needle Seat 238 Replace the Rotor Seal 241 Replace the Injection Valve 247 Remove the Metering Seal 252 Install the Metering Seal 257 Replace the Peristaltic Pump Cartridge 263 Replace the Flushhead Seal 266 Remove the Sample Loop-Flex 270 Installing the Sample Loop-Flex 274 Replace the Dummy Drawer 279 Replace the Sample Cooler/Sample Thermostat 287 Replace the Module Firmware 292

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