Honors Chemistry
Synthesis of 3a: The small amount of dense liquid remaining in the round bottom flask at this stage is 2 (2-bromo-3’-chloropropiophenone), which is a mild lachrymator (see Cautions above). Using a funnel, add to this flask, 10 mL of a 50:50 mixture of 5 mL t-butylamine and 5 mL of N-methylpyrrolidinone (NMP), and heat the flask in a 55-60°C ... ................
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